Coursehero >> Maine >> Bates >> ABACUS 218

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for Post-lab Experiment 2 Name: Date: Lab day: 1. 2. Solid unknown number: Draw the structure of solid unknown. 3. Actual m.p.: Lit. m.p.: Source: 4. Draw the structure of your unknown, and label the protons. Construct a table of the 1H NMR peaks below it. For each peak, give the chemical shift, integration, multiplicity, and peak assignment. 5. Draw the structure of your unknown, and label the carbons. Construct a table of the 13C NMR peaks below it. For each peak, give the chemical shift and peak assignment. 6. List the important IR peaks, and assign the bond vibrations 7. 8. Liquid unknown Draw number: the structure of liquid unknown. 9. Actual m.p.: Lit. m.p.: Source: 10. Draw the structure of your unknown, and label the protons. Construct a table of the 1H NMR peaks below it. For each peak, give the chemical shift, integration, multiplicity, and peak assignment. 11. Draw the structure of your unknown, and label the carbons. Construct a table of the 13C NMR peaks below it. For each peak, give the chemical shift and peak assignment. 12. List the important IR peaks, and assign the bond vibrations Attach the 1H and 13C NMR spectra, the IR spectra, and a copy of your notebook

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