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...224 CHEM M+W+F a.m. January 5, 2009 - Dr. Szpunar - 1 SYLLABUS CHEM 224 Organic Chemistry B 2nd semester Spring 2009 - LOYOLA UNIVERSITY CHICAGO (LUC) Lecture: Discussion: #1369 Section 007 #1370 Section 008 #1371 Section 009 M+W+F M M 10:25 a.m. 11:15 a.m. 12:35 p.m. 1:25 p.m. 1:40 p.m. 2:30 p.m. Flanner Hall 133 Damen 236 (may chng) Dumbach 227 (ditto) Sr. Lecturer: Dr. C. Szpunar Office: Flanner Hall 213 Emergency Message: Student Office Hours: Required: Contact: 773-508-3128,...
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224 CHEM M+W+F a.m. January 5, 2009 - Dr. Szpunar - 1 SYLLABUS CHEM 224 Organic Chemistry B 2nd semester Spring 2009 - LOYOLA UNIVERSITY CHICAGO (LUC) Lecture: Discussion: #1369 Section 007 #1370 Section 008 #1371 Section 009 M+W+F M M 10:25 a.m. 11:15 a.m. 12:35 p.m. 1:25 p.m. 1:40 p.m. 2:30 p.m. Flanner Hall 133 Damen 236 (may chng) Dumbach 227 (ditto) Sr. Lecturer: Dr. C. Szpunar Office: Flanner Hall 213 Emergency Message: Student Office Hours: Required: Contact: 773-508-3128, cszpuna@luc.edu Chemistry Dept. Office, 773-508-3100, fax: 773-508-3086 Tues: 11:30-12:15, Wed and Fri: 11:30-1:15, + by prior appt Organic Chemistry, Wade, L.G., Jr., 6th ed., Prentice Hall, 2003 (ISBN 0-13-147871-0). Suggested Materials: 1. Study Guide and Solutions Manual, Wade & Simek, 6th ed. (ISBN 0-13-147882-6), recommended. 2. Molecular modeling kit, Darling, Prentice-Hall, Freeman (Maruzen), Proteus, or equivalent. 3. Spiral or bound notebook for homework problems, recommended. Optional: Barron's Orgo Cards: Organic Chemistry Review, Steven Q. Wang, Babak Razani, Edward J.K. Lee, Jennifer Wu, and William Berkowitz (ISBN 0-7641-7503-3). Grading (approx weight below) with grade guidelines: > 90% A; 75-90% B; 55-75% C; grading may be curved EXAMS 2 dates announced (subject to change, although unlikely) NO MAKE UPS 40% UNEXCUSED ABSENCES merit a zero score. EXCUSED ABSENCES are handled on a case-by-case basis; grade weighting may be adjusted, depending on the circumstance(s); however, an excused absence MUST BE CORROBORATED and DOCUMENTED, e.g., accompanied by a note from the doctor, dentist, hospital rep, or funeral director; by a court summons; or by a plane ticket. QUIZZES TBD UNANNOUNCED (during lecture or discussion period or as take-home) 15% FINAL date announced (scheduled by CAS), no alternative date/time, NO MAKE UPS 45% Homework - assigned per chapter/topic, feel free to work any/all problems to apply and master concepts. Optional Short Report (as detailed below, one option ONLY) *** BONUS (maximum of 3 - 5%) Course Objective: To guide, encourage, and foster the learning and understanding of Organic Chemistry nomenclature, structures, properties, reactions, mechanisms, and syntheses by the individual student, helping him/her to connect, extrapolate, integrate, and apply the many different aspects learned. Student Outcomes: If successful, the student will learn how to 1. identify the various classes of organic compounds, their methods of preparation, and typical reactions. 2. name and draw specific organic compounds. 3. postulate a logical reaction mechanism for simple organic reactions. 4. discriminate amongst relative stabilities of reaction intermediates. 5. plan and write out multi-step syntheses using known functional group transformations. 6. prepare for basic purification/separation techniques of organic compounds required in the laboratory 7. analyze and interpret data from various instruments used in separating and identifying organic compounds: IR, NMR, and UV-vis spectrophotometers and mass spectrograph. CHEM 224 M+W+F a.m. January 5, 2009 - Dr. Szpunar - 2 Lecture and Discussion Attendance and Attention: Important and required. Feel free to bring your books and modeling kit to class. Better yet, use them. Prepare for lecture by prior scanning of new material. Come prepared for discussion, ready to ask questions on assigned homework or yet unassimilated lecture material. Phones and Pagers: Please be courteous and respectful of others. Silent mode during lecture and discussion. Not allowed in sight or within hearing during exams, subject to confiscation. NO phone conversations in lecture hall or in discussion class before class, during class, after class AT ANY TIME! Academic Honesty: Essential, expected, and enforced. Dishonesty dictates consequences which may include: (1) notification of Chemistry Department Chair, student s Department Chair, and CAS Dean, (2) documentation in the student s official university record, and (3) dismissal from the university. Immediate consequences will include a ZERO on any item in question (quiz or exam). Please refer to the LUC Undergraduate Handbook on policies or the CAS website: http://ww.luc.edu/cas/pdfs/CAS_Academic_Integrity_Statement_December_07.pdf). Study Strategies and Suggestions: One may approach the study of Organic Chemistry in a manner similar to tackling a new foreign language. Its study will provide a basis to understanding future material building constantly, incessantly, and relentlessly on the structural and mechanistic information presented previously. Over two semesters, the course will cover functional groups, aliphatic and aromatic compounds, bonding, nomenclature, stereochemistry, conformational analysis, reaction mechanisms, multi-step syntheses, and spectroscopy. Because the course is cumulative and builds heavily on prior material, the best plan is to study Organic Chemistry regularly, every day, similar to practicing the piano. Collaboration on homework problems is encouraged, especially in a timely fashion. Experience dictates that positive outcomes (for exam and course grades) are directly proportional to working and understanding the assigned problems on a regular basis, i.e., applying the concepts learned to non-generic compounds. Typically, Organic Chemistry is not efficiently self-taught. Overnight cramming will probably not success. produce The student should quickly read the chapter or segment to be covered BEFORE lecture to improve lecture comprehension. After lecture, careful detailed re-reading of the chapter or segment and focused working of the assigned problems are expected. If anticipating a passing grade of C, the minimal time per week devoted to Organic Chemistry is estimated at 4 hr for lecture/discussion, 3-6 hr for reading, and 3-6 hr for homework. Suggested Homework Assignment: Chap 15: Chap 16: Chap 17: Chap 18: Chap 19: Chap 20: Chap 21: Chap 22: Chap 23: Chap 24: Chap 25: Chap 26: 1, 4-18, 22-27, 30 3-4, 7-8, 9 (a,b), 12-29, 32, 38-39, 45 1-2, 4-22, 24-27, 30-32, 38, 40-52 1-4, 6-12, 16-31, 34-40, 43-44, 47, 49, 51 1-21, 25-32, 34-42, 44, 47, 56, 58 1-33, 35-40, 45, 47, 50 1-39, 43-48, 50-54, 66 1-47, 59-65, 67-69 1-14, 16-17, 21-22, 24-26, 28-31, 32 (a), 33-36, 40, 41 (a,b), 52-55, 63 3-6, 20, 32, 33 1, 4, 8-9, 11-15, 32 21-29 CHEM 224 M+W+F a.m. January 5, 2009 - Dr. Szpunar - 3 Optional BONUS Report CHEM 224, Spring 2009, Dr. Szpunar ***BE SURE to include on the cover sheet or top right of pg #1: a) your name b) the date c) CHEM 224 MWF d) lecturer s name ****************************************************************************************** Option 1 (max of 3%): Visit the International Museum of Surgical Science and write a 1-2 pp. report (of 12-pt type, 1-in margins, double-spaced, and stapled) highlighting at least 2 of its exhibits. Attach a pamphlet from the museum on one of its exhibits. You may wish to check to see if the # 151 Sheridan Bus (or equivalent) is more efficient than the CTA el; the bus may drop you closer to the museum, located just south of North Avenue Beach near the Polish Consulate on inner Lake Shore Drive. 1524 N. Lake Shore Drive Chicago, IL 60610 USA 312.642.6502, fax 312.642.9516, info@imss.org HOURS: May - September: Tuesday through Sunday 10 am 4 pm October - April: Tuesday through Saturday 10 am 4 pm ADMISSION: Adults $6, Students & Seniors $3 (Be sure to check the website for the current fee and free day!) _________________________________________________________________________________________ Option 2 (max of 5%): Choose a drug or health care product with articles, or a similar publication: organic functionalities featured in any of the following Chemical & Engineering News (C&E News), June 20, 2005, whole issue Top Pharmaceuticals, from aspirin to Viagra and more, approx. 50 pharmaceuticals. C&E News, Sept. 25, 2006, cover story Addiction smoking, drug, and alcohol abuse, pp. 21-44. C&E News, Oct. 30, 2006, cover story Biotechs , pp. 14-20. C&E News, Nov. 13, 2006, cover story RNA , pp. 16-23. C&E News, Oct. 2, 2006, cover story Mass Spectrometry proteins , pp. 17-25. C&E News, Oct. 23, 2006, cover story Bacterial Banter , pp. 17-26. C&E News, Dec. 4, 2006, cover story Pharm Year in Review, pp. 17-28. Write a 2-5 pp. report (of 12-pt type, 1-in margins, double-spaced, stapled, and including at least 3 pertinent references or citations at the end of the report). Include the following: Explain why the drug or health care product is of importance or interest to you. Identify all the functional groups from an organic perspective. Propose how you might verify the various functionalities spectroscopically, esp. via IR and NMR. Mention other methods, as applicable, i.e., via UV and MS. Suggest how you might change the molecule synthetically, at one functional site minimally, and state what you hope to achieve efficaciously by doing so. *** due on or before Monday, March 30, by 2 p.m. *** N.B.: Optional Bonus Report, either option, is intended for enrichment; points therefrom are only considered as a grade component IF student s interim grade is a C or better (i.e., >55% approx weighting). CHEM 224 M+W+F a.m. January 5, 2009 - Dr. Szpunar - 4 Lecture Outline (tentative, subject to change) Week 1 Date Jan 12 Jan 14 Jan 16 Jan 19 Jan 21 Jan 23 Jan 26 Jan 28 Jan 30 Feb 2 Feb 4 Feb 6 Feb 9 Feb 11 Feb 13 Feb 16 Feb 18 Feb 20 Chapter-Lec Topic *12 + 13* 15-1 15-2 *** 15-3 15-4 16-1 16-2 16-3 17-1 17-2 17-3 18-1 18-2 18-3 18-4 *** 18-5 19-1 19-2 19-3 *** 19-4 19-5 20-1 20-2 20-3 21-1 21-2 21-3 *** 22-1 22-2 22-3 *** 23-1 23-2 *** 23-3 23-4 24 25 26 Review IR, MS, NMR Conjugated Systems, UV Spectroscopy ************************************* Martin Luther King Holiday *** ***EVENT*** 2 3 Aromatic Compounds 4 Aromatic Compounds - Reactions 5 Ketones and Aldehydes 6 ************ WEDNESDAY ************ EXAM I (Chapters 15-18) 7 8 9 Feb 23 Feb 25(Ash W) Feb 27 Mar 2-6 Mar 9 Mar 11 Mar 13 Mar 16 Mar 18 Mar 20 Mar 23 Mar 25 Mar 27 Mar 30 Apr 1 Apr 3 Apr 6 Apr 8 Apr 9-13 Apr 15 Apr 17 Apr 20 Apr 22 Apr 24 Amines ********************************************* SPRING BREAK *** Carboxylic Acids 10 Carboxylic Acid Derivatives 11 *************************************** last day to withdraw *** Condensations and Alpha Substitutions of Carbonyl Compounds 12 *** Optional BONUS report due *** ************** FRIDAY ************* EXAM II (Chapters 19-22) Carbohydrates and Nucleic Acids ******************************** Good Friday, EASTER Monday *** 13 14 15 Amino Acids, Peptides, and Proteins Lipids Intro to Polymers 16 April 27 ******** Cumulative FINAL EXAM, Monday, 9 11 a.m., FH-133
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Loyola University of Chicago Proxy Vote History ISS Standard Rec For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For For Against For For For For For Record D...
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Loyola University of Chicago Proxy Vote History ISS Standard Rec For For For For For For For For For Record Date 10/3/2007 10/3/2007 10/3/2007 10/3/2007 10/3/2007 10/3/2007 10/3/2007 10/3/2007 10/3/2007 12/3/2007 12/3/2007 12/3/2007 12/3/2007 12/3/2...
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Loyola University of Chicago Proxy Vote History Record Date N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 2/10/2006 2/10/2006 2/10/2006 2/10/2006 2/10/2006 2/21/20...
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Loyola University of Chicago Proxy Vote History ISS Standard Catholic LUC Vote Cast Rec Policy Rec For For For For For For For For For For For For For For Against Against Against For For For For For For For For For For For For For For For For For For...
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
2008 ISA Undergraduate Student Paper Competition Submission Rules: 1. Maximum length of paper is 5,000 words, plus a 100-150 word abstract. 2. Paper must have been written for an undergraduate sociology course by an undergraduate at the time it was w...
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Subscribe to a Blackboard Podcast While you may listen to or view podcast episodes within Blackboard, the real benefit of podcasting is that podcasts can be subscribed to via RSS (really simple syndication). In Blackboard you have the option to subsc...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
Baumhart Hall Move-In Directions to Baumhart Hall (Address 26 East Pearson St, Chicago IL 60611) From the North: South on Lake Shore Drive (Hwy 41) Take Michigan Avenue exit and proceed to Chicago Avenue Right on Chicago Avenue proceed to State Stree...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
BAUMHART HALL PARKING INFORMATION 26 East Pearson Chicago IL 60611 Standard Parking 111 East Chestnut Garage Chicago, IL. 60611 312-640-1110 or 312-664-1198 3hrs or less-$15.00-$22.00 3hr to 10hrs--$25.00 10hrs to 24hrs-$31.00 Loyola Validations: In ...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
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Loyola Chicago >> WWW >> 1 (Fall, 2008)
CRISTO REY NETWORK FULL TUITION SCHOLARSHIP New Student Application 2009 - 2010 Loyola University Chicago invites students from Cristo Rey Network schools to apply to participate in the Cristo Rey Scholars Program. In order to be eligible for the sc...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
MARTIN J. SVAGLIC HUMANITIES SCHOLARSHIP New Student Application 2009 - 2010 A. Autobiographical Information Name: _ Social Security Number: _ E-mail address: __ I plan to enter Loyola Fall Year Male Female Spring _ I plan to major in: _ If no ma...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
JOHN T. TRAHEY MUSTARD SEED SCHOLARSHIP FOR THEATRE ARTS Loyola University Chicago Information and Application Audition Information and Tips All applicants are scheduled to arrive at 9 a.m. An audition order will be determined at that time. All in...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
The Accounting and Business Law (ABL) Department Scholarship Application This form should be used for applying for all ABL Area scholarships. Please check which scholarships you are applying for and be sure to provide all the appropriate documentatio...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
CURRICULUM VITAE JOHN J. KELLY Loyola University Chicago Department of Biology 6525 N. Sheridan Road Chicago, IL 60626 PROFESSIONAL INTERESTS Microbial Ecology Soil Microbiology Molecular Biotechnology EDUCATION Ph.D. Tel: 773.508.7097 Fax: 773....
Loyola Chicago >> WWW >> 1 (Fall, 2008)
Eects of an invasive cattail species (Typha glauca ) on sediment nitrogen and microbial community composition in a freshwater wetland Nicholas L. Angeloni1, Kathi Jo Jankowski1,2, Nancy C. Tuchman1,2 & John J. Kelly1 1 Department of Biology, Loyola...
Loyola Chicago >> WWW >> 1 (Fall, 2008)
ARTICLE IN PRESS Water Research 39 (2005) 32293238 www.elsevier.com/locate/watres DNA microarray detection of nitrifying bacterial 16S rRNA in wastewater treatment plant samples John J. Kellya, Slil Siripongb, John McCormacka,1, Lori R. Janusa, Hid...
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Elevated Atmospheric CO2 Alters Soil Microbial Communities Associated with Trembling Aspen (Populus tremuloides) Roots Lori R. Janus1, Nicholas L. Angeloni1, John McCormack1, Steven T. Rier1,2, Nancy C. Tuchman1,2 and John J. Kelly1 (1) Department of...
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JOURNAL OF CLINICAL MICROBIOLOGY, Aug. 2004, p. 37113730 0095-1137/04/$08.00 0 DOI: 10.1128/JCM.42.8.37113730.2004 Copyright 2004, American Society for Microbiology. All Rights Reserved. Vol. 42, No. 8 Use of 16S rRNA, 23S rRNA, and gyrB Gene Sequ...
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0038-075X/03/16809-597605 Soil Science Copyright 2003 by Lippincott Williams & Wilkins, Inc. September 2003 Vol. 168, No. 9 Printed in U.S.A. SOILS ISSUES MOLECULAR TECHNIQUES FOR THE ANALYSIS OF SOIL MICROBIAL PROCESSES: FUNCTIONAL GENE ANALYSIS ...
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Biol Fertil Soils (2003) 38:6571 DOI 10.1007/s00374-003-0642-1 ORIGINAL PAPER John J. Kelly Max M. Hggblom Robert L. Tate Effects of heavy metal contamination and remediation on soil microbial communities in the vicinity of a zinc smelter as ind...
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APPLIED AND ENVIRONMENTAL MICROBIOLOGY, May 2003, p. 28482856 0099-2240/03/$08.00 0 DOI: 10.1128/AEM.69.5.28482856.2003 Copyright 2003, American Society for Microbiology. All Rights Reserved. Vol. 69, No. 5 Optimization of Single-Base-Pair Mismatc...
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APPLIED AND ENVIRONMENTAL MICROBIOLOGY, Apr. 2003, p. 23772382 0099-2240/03/$08.00 0 DOI: 10.1128/AEM.69.4.23772382.2003 Copyright 2003, American Society for Microbiology. All Rights Reserved. Vol. 69, No. 4 Direct Proling of Environmental Microbi...
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ANALYTICAL BIOCHEMISTRY Analytical Biochemistry 311 (2002) 103118 www.academicpress.com Radical-generating coordination complexes as tools for rapid and eective fragmentation and uorescent labeling of nucleic acids for microchip hybridization John J...
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APPLIED AND ENVIRONMENTAL MICROBIOLOGY, July 2002, p. 32153225 0099-2240/02/$04.00 0 DOI: 10.1128/AEM.68.7.32153225.2002 Copyright 2002, American Society for Microbiology. All Rights Reserved. Vol. 68, No. 7 Parallel Characterization of Anaerobic ...
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APPLIED AND ENVIRONMENTAL MICROBIOLOGY, July 2002, p. 32153225 0099-2240/02/$04.00 0 DOI: 10.1128/AEM.68.7.32153225.2002 Copyright 2002, American Society for Microbiology. All Rights Reserved. Vol. 68, No. 7 Parallel Characterization of Anaerobic ...
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Soil Biology and Biochemistry 31 (1999) 14671470 www.elsevier.com/locate/soilbio Short communication Eects of the land application of sewage sludge on soil heavy metal concentrations and soil microbial communities John J. Kelly a, Max Haggblom b, ...
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Academic Program Development: Processes for Review, Approval & Implementation OFFICE OF THE PROVOST September 28, 2004 A. Academic Workflow As part of the flow of the academic work of the University, a variety of matters may arise that will require ...
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