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P60_H1
Course: P 60, Spring 2009School: Wisconsin
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P60 Unknown in CDCl3 Athena (Bruker-AC 300) 1H spectrum 10Hz/cm 10Hz/cm H3C N CH3 + 3.75 3.70 3.65 3.60 3.55 3.50 3.45 3.40 PPM 2.72 2.70 2.68 2.66 PPM H CH2 20Hz/cm 3.04 10Hz/cm 2.1 2.0 1.9 1.8 1.7 PPM 5.04 7.35 7.30 7.25 7.20 7.15 PPM 2.11 2.99 2.05 2.08 2.00 8 7 6 5 4 3 1.04 2 2.02 1 0 PPM
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P60 Unknown in CDCl3 Athena (Bruker-AC 300) 1H spectrum
10Hz/cm 10Hz/cm
H3C N
CH3
+
3.75 3.70 3.65 3.60 3.55 3.50 3.45 3.40 PPM 2.72 2.70 2.68 2.66 PPM
H
CH2
20Hz/cm 3.04 10Hz/cm
2.1
2.0
1.9
1.8
1.7
PPM
5.04
7.35
7.30
7.25
7.20
7.15
PPM
2.11 2....
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030124_21 59 (1.091) Cm (57:78-200:220) 100361.1B14 in methanol LCT S. Przybylinski699.1TOF MS ES+ 2.77e4%700.2 362.1 701.202002503003504004505005506006507007508008509009501000m/z030124_21 59 (1.091)
Wisconsin - A - 11
Unknown A11 in CDCl3 INOVA-600 gcosy 1H COSY spectrumF2 (ppm) 1.2 1.47a 7b-OH 10b 12b 6 12a 10a 11a 3a 11b15 3b 2a 2b161024x256 FT'd to 1024x1024 sinebell-squared apodization symmetrized11 12 10 9 8 7 61.6 1.8 2.0 2.2 2.4 2.6 2.8H3C3
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E03 (E:A-03) in CDCl3 orginally labelled E05 Athena Automation run Jan 16, 2003 D. Mowrey8.07.87.67.47.27.06.8PPMExpansions are 20 Hz/cmCH3OCH3HOO2.22.12.01.91.8PPM4.40 1.994.34PPM 3.00 3.011.981.98 2
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Unknown O13 in CDCl3 Athena (Bruker-AC 300) 1H spectrumO O CH3all expansions at 20Hz/cmOCH33.43.33.23.1PPM2.952.012.020.990.981.00 1.001.962.018.07.97.87.77.67.57.44.36 4.32 PPM 4.38 4.34 4.30 PPM2.
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Unknown O13 in CDCl3 Athena (Bruker-AC 300) 1H spectrumO O CH3all expansions at 20Hz/cmOCH33.43.33.23.1PPM2.952.012.020.990.981.00 1.001.962.018.07.97.87.77.67.57.44.36 4.32 PPM 4.38 4.34 4.30 PPM2.
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Unknown O42 in CDCl3 Athena (Bruker-AC 300) 1H spectrumCH3 O OO2.25 2.20 2.15 2.10 2.05 2.00 1.95 1.90 PPM3.5 8.1 8.0 7.93.063.42.993.33.23.1PPM7.87.77.6PPM3.002.00all expansions at 20Hz/cm1.07 1.051.041.041.00
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Unknown O42 in CDCl3 Athena (Bruker-AC 300) 1H spectrumCH3 O OO2.25 2.20 2.15 2.10 2.05 2.00 1.95 1.90 PPM3.5 8.1 8.0 7.93.063.42.993.33.23.1PPM7.87.77.6PPM3.002.00all expansions at 20Hz/cm1.07 1.051.041.041.00
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Unknown O10 in CDCl3 Athena (Bruker-AC 300) 13C spectrum180 160169.844CH2O O C140CH3120 100 80148.982 132.341 130.753 130.696 130.498 130.047 129.923 128.757 128.165 128.005 127.490 126.866 126.611 126.553 123.311 121.414 121.297 115.
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Unknown O10 in CDCl3 Athena (Bruker-AC 300) 13C spectrum180 160169.844CH2O O C140CH3120 100 80148.982 132.341 130.753 130.696 130.498 130.047 129.923 128.757 128.165 128.005 127.490 126.866 126.611 126.553 123.311 121.414 121.297 115.
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Unknown H82 (H:E-02) in CDCl3 Athena Automation 300MHz cgfryinteg=.75 exp=200Hz/cmall other expansions 20Hz/cm2.9 13.0 12.5 12.0 11.5 11.0 10.5 10.0 PPM2.82.72.62.52.42.32.22.1PPM3.55 3.50 3.45 3.40 3.35 3.30 3.25 PPM8.0
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Unknown H82 (H:E-02) in CDCl3 Athena Automation 300MHz cgfryinteg=.75 exp=200Hz/cmall other expansions 20Hz/cm2.9 13.0 12.5 12.0 11.5 11.0 10.5 10.0 PPM2.82.72.62.52.42.32.22.1PPM3.55 3.50 3.45 3.40 3.35 3.30 3.25 PPM8.0
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Unknown B05 NOESY1D data from INOVA-600, H15 selectedmix=1s, d1=10s, nt=16H1320 1H9H8 7H12 11 16 152 3 4 18 1710 5 6O191714H H14HHH158.07.87.67.47.27.06.86.66.4ppm3.63.43.2
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Unknown B05 NOESY1D data from INOVA-600, H15 selectedmix=1s, d1=10s, nt=16H1320 1H9H8 7H12 11 16 152 3 4 18 1710 5 6O191714H H14HHH158.07.87.67.47.27.06.86.66.4ppm3.63.43.2
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Unknown Y26 in CDCl3 Hermes (Mercury-300) 1H spectrumdataset: ta_Y26_146_17_02HN+Cl-2.82.62.42.22.01.8PPMall expansions at 20 Hz/cm1.41.31.21.11.00.9PPM7.75 7.70 7.65 7.60 7.55 7.50 7.45 7.40PPM2.902.9
Wisconsin - C - 636
Unknown Y26 in CDCl3 Hermes (Mercury-300) 1H spectrumdataset: ta_Y26_146_17_02HN+Cl-2.82.62.42.22.01.8PPMall expansions at 20 Hz/cm1.41.31.21.11.00.9PPM7.75 7.70 7.65 7.60 7.55 7.50 7.45 7.40PPM2.902.9
Wisconsin - C - 24
Unknown L24 in CDCl3 Athena (Bruker-AC 300) 1H COSY spectrum512x128 FT'd to 512x512 sinebell-squared apodization symmetrizedO OC2H5PPM F2H3C HC H3C O6NO NO 258765 PPM F14321874321
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201.857Unknown A07 in CDCl3 Athena (Bruker-AC 250) 13C spectrum200O OEt COOH174.521 173.128150140.929 135.660 131.499 128.917 128.255 127.195 126.824 124.899 124.030 123.79810093.132CDCl3 refed to 77.25ppm77.760 77.250 76.74364.29
Wisconsin - A - 636
77.673 77.250 76.82642.82736.357179.065Unknown A09 in CDCl3 Athena (Bruker-AC 250) 13C spectrumH3C CH CH2COOH145.653128.796 126.928 126.738CDCl3 ref'ed to 77.25ppm2001501005022.0700PPM
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Unknown A10 in CDCl3 Athena (Bruker-AC 250) 13C spectrum180MeO172.260160 140159.793141.532 137.744CH3O126.656 126.481 126.301 124.710 119.295120 100 80 60 40 20 PPMCH2 C O OCH3CDCl3 ref'ed to 77.25ppm107.16577.673 77.250 76
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030124_20 60 (1.100) Cm (60:74-177:196) 239.1 100F80 in methanol LCT S. PrzybylinskiTOF MS ES1.55e4%240.1 237.1 479.20150200250300350400450500550600650700750m/z030124_20 60 (1.100) Cm (60:74-177:196) 100239.1
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030124_18 54 (0.990) Cm (49:71-124:152) 297.0 100H82 in methanol LCT S. PrzybylinskiTOF MS ES8.36e4%298.1595.1596.2 655.40200225250275300325350375400425450475500525550575600625650675700725750
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