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6 TsNH2, Experiment BF3 Et2O PhCHO benzene, Dean-Stark Ph N . Ts To a solution of benzaldehyde (1.59 g, 15 mmol) and p-toluenesulfonamide (2.57 g, 15 mmol) in benzene (100 mL) was added BF3Et2O (0.12 mL). The mixture was refluxed on a Dean-Stark apparatus for 24 h. The cooled solution was poured into saturated NaHCO3 (100 mL), the benzene layer was isolated, and the water layer was extracted with ethyl acetate...
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TsNH2, Experiment BF3 Et2O PhCHO benzene, Dean-Stark Ph N
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Ts
To a solution of benza...
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UCLA - CHEM - 136
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Colorado - AMATH - 2360
Colorado - AMATH - 2360
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