St. Thomas - MMSE - 621

DYNAMYTE PROGRAMMING WORKSTATIONFeatures Commands Setup and UseFeaturesDynaMyte 2800 CNC Machining Tool Dyna 2800 C Controller Spindle speeds Designed to run from 200 to 5000 rpm Will run at 0 - 10,000 rpm 0 - 3750 rpm 0 - 2000 rpm determined by

Toledo - STA - 447

Toledo - STA - 447

Toledo - STA - 447

Arizona - ECE - 430

Arizona - ECE - 220

Lecture 3 Goals:Lab Practical (First Hour of Lab, 70 Pts.) Estimation of Thevenin, Norton Parameters Constant Current Source Thevenin Equivalent of Transistor Dimmer1Lab Practical ChecklistBreadboard a circuit consisting of resistors, tran

Michigan - CHEM - 216

The University of Michigan Chemistry 216HWinter Term, 2005Class MeetingsSection 210 211 220 250 290 291 Day M M Tu W F F Time 1-5 pm 1-5 pm 8-12 pm 1-5 pm 1-5 pm 1-5 pm Room 2411 2500 2500 2500 2411 2500 GSI Erin Fuller Nick Deprez Mike Bury Nick

Michigan - CHEM - 216

Notebook Check (Experiment 1) Name:_ Ready for todays lab No mixed experiments; Continued on and continued from Date all entries For one of the randomly selected experiments: (a) the molecular equation for the intended reaction (b) table of physical

Michigan - CHEM - 216

Name _Date_Write-up for Experiment 1Write up a journal style experimental including characterization. (10 points)Experimental (10) Experimental are written correctly in content and style; publishable Journal-style experimental text (8) Experime

Michigan - CHEM - 216

Your section: Your group members names: Name of proposal: Criteria The proposal is organized (clearly written, easy to follow, well referenced) The proposal is well grounded in the literature (We are convinced that the final product can be made.) The

Michigan - CHEM - 216

IR stretches you will be responsible for knowing such that you should be able pick them on an IR spectrum OH 3600 -2500 NH 3500- 3300 CH sp 3300 CH sp2 3080-3020 CH sp3 2960-2850 C(=O)H aldehyde 2 peaks 2900, 2700 CC/CN 2260-2150 C=O 1750-1650 C=C 16

Michigan - CHEM - 216

Laboratory NotebooksRegardless of whether an individual works in one of the traditional scientific professions, or in art, or in writing, a personal diary of activities known as a "notebook" or a "journal" plays an important role. In chemistry, labo

Michigan - CHEM - 216

Notebook Check: Ready for today's labName:_ _1 _1 _1 _1 _2No mixed experiments; "Continued on" and "continued from" Date all entries For one of the randomly selected experiments: (a) the molecular equation for the intended reaction (b) table of p

Michigan - CHEM - 216

The Scientific LiteratureHonors Cup 2005 1/13/05General 216 Announcements Office Hours: 3:30-5:00 2404 Thursdays GSI "office hours" Post experiment 1 details ~5pm on Friday at: http:/www.umich.edu/~chemh215/CHE M216/216Hhome.htm NMRThe Honor

Michigan - CHEM - 216

Experiment 1: Friedel-Crafts AcylationBackground: Goals: a) work with water-sensitive reagents; b) design experimental procedure and work-up; and c) to assess the procedural design. Electrophilic aromatic substitution reactions take place between th

Michigan - CHEM - 216

Experiment 2: Two-step Synthesis of Ethyl 4-MethoxycinnamateBackground Why is ethyl 4-methoxycinnamate (1) interesting? First, it is the analog of octyl 4-methoxycinnamate (2), a UV light blocker found in Bain de Soleil All Day Sunblock and Copperto

Michigan - CHEM - 216

Experiment 3: Diels-Alder exo or endo?Background A Diels-Alder cycloaddition reaction can result in either and/or both endo and exo-products. Does the neat Diels-Alder reaction of furan with N-phenylmaleimide produce exo and/or endo-7oxabicyclo[2.2.

Michigan - CHEM - 216

Honors Cup Progress Report (name, section) Introduction What synthesis are you doing? Step X: Synthesis of _ I. Progress Summary Reaction scheme (draw the reaction) Table 1: Step X (Put checks in the boxes that you have completed) Reactant 1 Reactant

Michigan - CHEM - 216

Name: _Date:_Weekly reflectionOn a scale from 1 to 10, rank how well you feel your previous lab went. Did not go as expected 1 2 3 4 5 6 Went exactly as expected 7 8 9 10(a) Briefly describe, being as specific as possible, why you chose the ra

Michigan - CHEM - 216

A version of the procedure: Aluminum chloride is water sensitive, an irritant, and corrosive. It will react with the moisture on your skin to liberate HCl. Handle it with care, weigh out only what is necessary, and work quickly but safely. Acetyl chl

Michigan - CHEM - 216

Supplemental MaterialTitle: A Discovery-Based Friedel-Crafts Acylation Experiment: Student-Designed Experimental ProdedureAuthor: Anne McElwee Reeve, Chemistry Program, School of Science, Lynchburg College, Lynchburg, VA 24501Lab Documentation

Michigan - CHEM - 216

Working up NMR spectra in the SLCWhen taking your data on the NMR: 1) Make note of the file name and the file directory under which you save your spectrum 2) Make sure you know the 216H (or other class) login and password for the console at the NMR

Michigan - CHEM - 216

NMR Spectroscopy: Preparing a Sample Background Reading Derome, A.E. Modern NMR techniques for chemistry research; Pergamon Press: Oxford, 1987. Harris, R.K. Nuclear Magnetic Resonance Spectroscopy; Longman: Essex, 1986. Hornak, J.P. Basics of NMR, h

Michigan - CHEM - 216

Notes on using the Bruker AC-200- TECMAG 200MHz NMRPrecautions: WARNING! Remove your wallet, watches, etc. before approaching the magnet! Never bring any ferromagnetic items into the magnet room. Be careful with metal objects in the room. Avoid tak

Michigan - CHEM - 216

4230J . Org. Chem. 1987,52, 4230-4234An Assessment of the Causes of the "Cesium Effect"Gerard Dijkstra, Wim H. Kruizinga, and Richard M. Kellogg*Department of Organic Chemistry, University of Groningen, Nijenborgh 16, Groningen 9747 AG, T h e N

Michigan - CHEM - 216

In the Laboratoryedited byThe Microscale LaboratoryR. David CrouchDickinson College Carlisle, PA 17013-2896Two-Step Semi-Microscale Preparation of a Cinnamate Ester Sunscreen AnalogWRyan G. Stabile and Andrew P. Dicks* Department of Chemi

Michigan - CHEM - 216

SUPPLEMENTAL INFORMATION Lab Documentation For On-Line Publication Two-Step Semi-Microscale Preparation Of A Cinnamate Ester Sunscreen AnalogRyan G. Stabile and Andrew P. Dicks* Department of Chemistry, University of Toronto, 80 St. George Street,

Michigan - CHEM - 216

Name:_Date:_On a scale from 1 to 10, rank how well you feel your previous lab went. Did not go as expected 1 2 Went exactly as expected 8 9 1034567(a) Briefly describe, being as specific as possible, why you chose the ranking that you

Michigan - CHEM - 216

In the Laboratoryendo- and exo-Stereochemistry in the DielsAlder Reaction: Kinetic versus Thermodynamic Control1James H. Cooley and Richard Vaughan Williams Department of Chemistry, University of Idaho, Moscow, ID 83844-2343 In these experiments,

Michigan - CHEM - 216

Experiment 3: Diels-Alder exo or endo? Background A Diels-Alder cycloaddition can result in either and/or both endo and exo- products. Does the neat Diels-Alder reaction of furan with N-phenyl maleimide produce exo and/or endo-7oxabicyclo[2.2.1]hept-

Michigan - CHEM - 216

Experiment 2: Two step synthesis of ethyl 4-methoxycinnamate Background Why is ethyl 4-methoxycinnamate (1) interesting? First, it is the analog of octyl 4-methoxycinnamate (2), a UV light blocker found in Bain de Soleil All Day Sunblock and Copperto