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UCSD | CHEM CHEM 6BL
CHEM 6B LAB
Professors
- Berniolles,
- Bernoillles,
- Bernoilles,
- Bernouilles,
- Borniolles,
- Berniolis
59 sample documents related to CHEM CHEM 6BL
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CHEM 6BL EXPERIMENT 1 ANSWER KEY PRELAB & POSTLAB QUESTIONS PRELABORATORY QUESTIONS 1. The steps are: OxH Ox + H+ Al3+ + 3 Ox Al(Ox)3 (s) 2. 0.01000 M (four sig. figs.) 3. Al3+ 4. 0.0017 excess moles Ox added 5. See explanations in lecture notes 6. Averag
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CHEM 6BL EXPERIMENT 2 ANSWER KEY PRELAB 250 mL) water, and then add water to the calibration mark in a 2
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CHEM 6BL EXPERIMENT 3 ANSWER KEY PRELAB & POSTLAB QUESTIONS PRELABORATORY QUESTIONS 1. See MSDS Information 2. Not required this quarter 3. Cc = 8.78 J/K 4. Tfinal = 21.14C 5. 99.8 kJ 6. Tf = 38.9C POSTLABORATORY QUESTIONS 1. Not required this quarter 2.
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Department of Chemistry & Biochemistry, University of California, San Diego CHEM 6BL Full Paper Laboratory Report Writing Guide: Experiments 4A-C JOURNAL ARTICLE REFERENCE: ORGANOMETALLICS PAPER POSTED ON WEBCT Specific instructions on what to include and
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EXPERIMENT 4A ANSWER KEY PRELAB & POSTLAB QUESTIONS PRELABORATORY QUESTIONS 1. 1 Fe(NH4)2(SO4)26H2O + 1 H2C2O4 1 FeC2O4 + 2 NH4+ + 2 SO42- + 2 H+ + 6 H2O Not a redox reaction 2. 0.00293 mol 3. 0.0060 mol 4. Fe(NH4)2(SO4)26H2O 5. 0.422 g 6. See lecture not
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Undergraduate Laboratory Safety Exam STUDY GUIDE Biochemistry University of California, San Diego Contents INTRODUCTION . 4 1. LAB RULES & BASIC LAB PRACTICES . 5 LAB RULES
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APPENDIX B Spectrometry When white light is allowed to pass through a prism, the light is diffracted into a spectrum of colors. This spectrum of colors has a range of wavelengths varying from 400 nm (violet) to 700 nm (red) and is referred to as the visib
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EXPERIMENT 1 Gravimetric Analysis INTRODUCTION Analytical Chemistry: Gravimetric Analysis Analytical chemistry is perhaps the most fundamental branch of chemistry as it involves either identifying the components that make up a compound or determining the
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EXPERIMENT 2 Volumetric Analysis of an Organic Acid INTRODUCTION Analytical Chemistry: Volumetric Analysis In Experiment #1, the concentration of a solution of aluminum ion was determined by gravimetric analysis. Although still a commonly used method for
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EXPERIMENT 3 Thermochemistry INTRODUCTION Heat exchange is one of the most common processes explored in the chemical laboratory. The examination of the relationships between heat energy and chemical changes is called thermochemistry. If heat energy is rel
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EXPERIMENT 4C Analysis of Iron in an Iron(III) Oxalate Complex INTRODUCTION Spectrophotometry In the previous experiment, an iron(III) oxalate complex was analyzed for its oxalate content. In this experiment, the iron content in this complex will be deter
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EXPERIMENT 5 Semimicro Qualitative Analysis INTRODUCTION A complete chemical analysis of a sample focuses first on what is in the sample (a systematic study called qualitative analysis). Once the chemist knows which substances are present, then a quantita
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EXPERIMENT5 SEMIMICROQUALITATIVEANALYSIS PARTII FLOWCHARTANALYSIS CHEM 6BL Qualitative Analysis Photo Gallery Page 1 Procedure 1: known Procedure 1: unknown Procedure 2 known: positive test for Hg2(2+) Procedure 2 unknown: negative test for Hg2(2+) CHEM 6
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EXPERIMENT 6 Atomic Spectra INTRODUCTION Visible light is the portion of the electromagnetic radiation spectrum to which the eye is sensitive. Figure 1 indicates that visible light is only a narrow band of electromagnetic radiation. Any portion of this ra
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CHEM 6BL. Introductory Inorganic Chemistry Laboratory 1 Sandrine Berniolles, Ph.D. Department of Chemistry & Biochemistry Course Site: WebCT Office Location: York 4030A E-Mail: sberniolles@ucsd.edu Specify name/section # in subject line! Office Hours: Ins
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1 Experiment #1 Gravimetric Analysis Analytical Chemistry 2 Fundamental branch of Chemistry that involves separating, identifying, and determining the relative amounts of the components in a sample of matter Qualitative Analysis: Identifying the chemical
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1 Experiment #2- Parts I-II Volumetric Analysis of an Organic Acid Volumetric Analysis 2 Known volumes of known concentrations are reacted with known volumes of unknowns From reaction equation, relate to moles Common analytical technique: titration with
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1 Experiment #2- Parts III-V Volumetric Analysis of an Organic Acid Experiment 2 Overview 2 Parts I-II. Preparation/standardization of NaOH titrant solution Part III. Determination of the molar mass of an unknown acid by acid unknown acid by acid-base ti
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1 Experiment #3 Thermochemistry Thermochemistry 2 Thermochemistry is the study of heat changes that take place in a change of state or a chemical reaction Heat energy is either absorbed or released energy is either absorbed or released Exothermic process
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CHEM 6BL Experiment 4A: Iron Oxalate Complex Synthesis Instructor: Dr. S. Berniolles Experiment #4 Concepts Complex Chemistry Stoichiometry: Limiting Reagent & % Yield Redox React
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CHEM 6BL Experiments 4B-C: Iron Oxalate Complex Analysis Instructor: Dr. S. Berniolles Experiment 4A Synthesis Fe2+ 2 SO42- = 4- Fe(NH4)2(SO4)26H2O 2 NH4+ = 2+ NH K+ Kw [Fex(C2O4)y]zH2O Fe3+ C2O421 Inorganic Complex Synthesis Product 2 EXAM S EXAM #1 IN
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CHEM 6BL Experiment 5: Qualitative Analysis Instructor: Dr. Sandrine Berniolles Analytical Chemistry Fundamental branch of Chemistry that involves separating, identifying, and determining the relative amounts of the components in a sample of matter of mat
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Department of Chemistry & Biochemistry, University of California, San Diego CHEM 6BL EXPERIMENT 1 LAB REPORT WORKSHEET Gravimetric Analysis Author: _ Date: _ TA Name/Lab Section No.: _ TA/Grader Only: Graded Components Prelab Procedure (graded by TA) P
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Department of Chemistry & Biochemistry, University of California, San Diego CHEM 6BL EXPERIMENT 2 LAB REPORT GRADE SHEET Volumetric Analysis Author: _ Date: _ TA Name/Lab Section No.:_ For the purpose of grading the accuracy of your results, report the f
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Department of Chemistry & Biochemistry, University of California, San Diego CHEM6BLEXPERIMENT3LABREPORTGRADESHEET Thermochemistry Author: _ Date: _ TA Name/Lab Section No.:_ Important Note: This lab report is a short report: The introduction and Experime
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CHEM 6BL Experiments 4A-C Lab Report Grade Sheet Department of Chemistry & Biochemistry, University of California, San Diego Synthesis and Analysis of an Iron(III)-Oxalate Complex Author: _ Date: _ TA Name/Lab Section No.:_ For the purpose of grading the
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CHEM 6BL Experiment 5 Lab Report Grade Sheet Department of Chemistry & Biochemistry, University of California, San Diego Semimicro Qualitative Analysis Author: _ Date: _ TA Name/Lab Section No.:_ For the purpose of grading the accuracy of your results, re
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Chemistry 6BL Syllabus Introductory Inorganic Chemistry Laboratory Summer Session I, 2010 INSTRUCTOR: OFFICE LOCATION: Dr. Sandrine Berniolles York Hall 4030A-3 E-mail: sberniolles@ucsd.edu (IMPORTANT: Please specify your name & lab section # in the subje
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VolumeofNaOHTitrantvs.pH 14.00 12.00 10.00 8.00 pH 6.00 4.00 2.00 0.00 0.00 5.00 10.00 15.00 20.00 25.00 30.00 35.00 VolumeofNaOHTitrant(mL) VolumeofNaOHTitrantAdded(mL) 0 3.2 7 11.12 15 17.9 19.72 20.8 21.35 21.65 21.8 21.9 21.95 22 22.03 22.1 22.13 23.2
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Time 1 2 3 4 5 6 6.5 7 7.5 8 8.5 9 9.5 10 Temp 10 10 10.5 10.5 10.5 41 41 41 41 40.9 40.5 40.1 40 39.9 41 41 41 41 40.9 40.5 40.1 40 39.9 Timevs.TemperaturefortheDeterminationoftheCalorimeterConstant,Cc(J/K) 55.00 50.00 45.00 f(x) = -0.32x + 43.19 40.00 3
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Graph#1ConcentrationatComplexasafunctionofAbsorbance(Beer\'sLawCalibration) 0.600 f(x) = 5924.7x + 0 R = 1 5; 0.53 0.500 0.400 4; 0.38 Absorbance 0.300 3; 0.23 0.200 2; 0.15 0.100 0.000 0 0 0 0 0 0 0 0 0 ConcentrationFe(bipy)(M) Graph#1ConcentrationatCompl
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CHEM 6BL PRACTICE FINAL EXAM IMPORTANT STUDY RECOMMENDATIONS In order to be best prepared for your upcoming final exam, which covers experiments 4A-6, make sure you review the following items: Pre- and postlab questions Lecture notes and exercises include
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CHEM 6BL PRACTICE EXAM #1 IMPORTANT STUDY RECOMMENDATIONS In order to be best prepared for your upcoming midterm, which covers experiments 1-4A, make sure you review the following items: Pre- and postlab questions Lecture notes and exercises included in t
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Chemistry 6BL - PRACTICE FINAL EXAM Spring Quarter 2009 IMPORTANT STUDY RECOMMENDATIONS To be well prepared for your upcoming final exam, which covers experiments 4B-6, make sure you review the following items: Pre- and postlab questions Lecture notes and
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6 BL Midterm #1 KEY: Spring 2009 - Form A 1) B 2) C 3) B 4) B 5) E 6) D 7) B 8) B 9) B 10) E 11) B 12) C 13) E Page 1
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6 BL Midterm #1 KEY: Spring 2009 - Form B 1) E 2) B 3) B 4) C 5) B 6) B 7) D 8) B 9) C 10) C 11) E 12) E 13) B Page 1
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CHEM 6BL Experiments 1-3 Guide EXPERIMENT 1 GUIDE Gravimetric Analysis In this experiment, students precipitate the Al3+ ion in a solution of unknown concentration by reacting it with an organic anion, 8-hydroxyquinolinate, forming a solid complex of alum
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Chem 6BL Experiments 4A-C Practical Guide EXPERIMENT 4A Synthesis of an Iron (III) Oxalate Complex In this experiment, you will synthesize a coordination compound Kw[Fex(C2O4)y]zH2O in which iron (III) coordinates with oxalate ion, the anion of a diprotic
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Chem 6BL Experiments 5-6 Practical Guides EXPERIMENT 5 GUIDE Semimicro Qualitative Analysis In this experiment, you will investigate a mixture of nine common metal ions (Ag+, Hg22+, Cu2+, Bi3+, Mn2+, Fe3+, Ni2+, Cr3+, and Zn2+). In Part I, you will study
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UCSD Chemistry fire extinguisher Know the hazards of the materials to be used Check for a current certification sticker Ver
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EXPERIMENT 5 SEMIMICRO QUALITATIVE ANALYSIS PART II FLOW CHART ANALYSIS Procedure 1: known Procedure 1: unknown Procedure 2 known: positive test for Hg2(2+) Procedure 2 unknown: negative test for Hg2(2+) Procedure 3 known: positive test for Ag+ Procedure
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CHEM 6BL PRELAB/POSTLAB ANSWER KEY EXPERIMENT #4B: ANALYSIS OF OXALATE LIGANDS IN AN IRON (III) OXALATE COMPLEX PRELAB ANSWER KEY 1. (2 points) 2 MnO4 + 5 H2C2O4 + 6 H+ 2 Mn2+ + 10 CO2 + 8 H2O 2. (2 points) 0.09823 M KMnO4 3. (2 points) 0.7062 mmol of C2O
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CHEM 6BL PRELAB/POSTLAB ANSWER KEY EXPERIMENT #5: SEMIMICRO QUALITATIVE ANALYSIS PRELAB ANSWER KEY 1. (0 point) See MSDS Information. 2. (0 point) See MSDS Information. 3. (2 points) + Ag Hg22+ Cu2+ Bi3+ Sn4+ Fe3+ Mn2+ Zn2+ Ni2+ Cr3+ ClInsol/Prec Insol/Pr
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Laboratory Notebook #6 must be completed using a customized laboratory report worksheet. Read the worksheet carefully to see which sections of the lab report need to be written-up by hand
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Lab Report Guide for Experiments #4A-C \"Full Paper\" Report Basic formatting Guidelines: The \"full paper\" report for Experiments #4A-C MUST be typed up/printed out Font Size: 12 points Paragraph Spacing: Single-spaced, or 1 and 1/2-spaced Columns: NOTE -
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4938 Organometallics 2003, 22, 4938-4946 Synthesis and Characterization of Metal Complexes Possessing the 5-(2-Pyridyl) Pyrazolate Ligands: The Observation of Remarkable Osmium-Induced Blue Phosphorescence in Solution at Room Temperature Pei-Chi Wu, Jen-K
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UCSD Chemistry & Biochemistry Undergraduate Teaching Laboratories laboratory safety exam SPRING 2009 CHEM 6BL, 100A and 143A ALL students in these introductory lab classes are required to demonstrate an understanding of general laboratory safety and the U
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Undergraduate Laboratory Safety Exam STUDY GUIDE Biochemistry University of California, San Diego TABLE OF CONTENTS Section INTRODUCTION. 1 2 LABORATORY RULES & BASIC LAB PR
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CHEM 6BL Experiment 5: Qualitative Analysis Instructor: Dr. Sandrine Berniolles Chemistry 6BL Lab/Course Schedule Week of May 11 Lecture & Lab Lab Exam Period Schedule Schedule Qualitative 1st lab End Experiment 4C Analysis (Expt. 5) 2nd lab Expt. 5 (Part
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CHEM 6BL Experiment 6: Atomic Spectra Instructor: Dr. Sandrine Berniolles CHEM 6BL Course Schedule Date Lecture Lab Report Due Dates May M 2727-28 June 1 -3 - 2nd lab E d E t 5/St t l b End Expt. 5/Start Expt.
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LAB REPORT FORMAT (BASICS) Below is a basic description of the CHEM 6BL lab report format requirements. Refer to the CHEM 6BL Lab Manual- General Information Report Guide posted on WebCT for a more detailed
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CHEM 6BL Experiment 2: Volumetric Analysis of An Organic Acid Instructor: Dr. S. Berniolles Safety Exam Schedule Reminders If you failed or missed the safety exam: makeup on Thursday, Oct. 9, 7 am in York 2722 (Safety Contact: Sheila Kennedy 858-534-0221)
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CHEM 6BL Experiment 1: Gravimetry Dr. Sandrine Berniolles Experiment 1: Gravimetric Analysis Analytical Chemistry: Fundamental branch of chemistry that involves either: o Identifying the components that make up a compound (qualitative analysis) o Determin
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Ian J. Ball Chemistry 6BL: Introductory Inorganic Chem. Lab. Introductory Chem Ian J. Ball, Ph.D. Department of Chemistry 11-12pm; W, 10:30-12:00; Th, 1
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Ian J. Ball Chemistry 6BL: Introductory Inorganic Chem. Lab. Introductory Chem Ian J. Ball, Ph.D. Department of Chemistry 11-12pm; W, 10:30-12:00; Th, 1
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