• 19 Pages nitrationofmethylbenzoate
    Nitrationofmethylbenzoate

    School: George Mason

    Course: Organic Chemistry Lab II

    Nitration of Methyl Benzoate Overview: Synthesis Nitration of Methyl Benzoate through an Electrophilic Aromatic Substitution to form Methyl m-Nitrobenzoate (MW 181.15). Determination of reactant Masses, Moles, Molar Ratio, Theoretical Yield Reac

  • 133 Pages NMRlecture
    NMRlecture

    School: George Mason

    Organic Chemistry Laboratory BuildingAToolset For TheIdentificationofOrganicCompounds PhysicalProperties MeltingPoint BoilingPoint Density Solubility RefractiveIndex 04/22/12 ChemicalTests Hydrocarbons Alkanes Alkenes Alkynes Halides Alcohols Aldehydes Ke

  • 23 Pages nitrationofmethylbenzoate
    Nitrationofmethylbenzoate

    School: George Mason

    NitrationofMethylBenzoate Demonstrationoftheeffectofanelectronwithdrawing grouponamonosubstitutedbenzeneringon subsequentsubstitutionofothergroupsontheBenzene ring References: 04/22/12 Pavia,etal. pp352357 Slayden,etal. pp6769 1 NitrationofMethylBenzoate

  • 16 Pages isopentylacetate
    Isopentylacetate

    School: George Mason

    SynthesisofIsopentyl(Amyl)AcetateEster (BananaOil) Overview SynthesisAcid(H2SO4)catalyzedFischerEsterification reactionofaCarboxylicAcid(AceticAcid)withtheHydroxyl groupofanAlcohol(Isopentyl[amyl]Alcohol). ThisisaCondensationreactionwherethemoleculesbecom

  • 35 Pages grignardbenzoicacid(sonication)
    Grignardbenzoicacid(sonication)

    School: George Mason

    GrignardReagent/Reactions PreparationofaGrignardReagent (Phenylmagnesiumbromide)andreactionwith CarbonDioxidetoformBenzoicAcid throughanElectrophilicAdditionreaction References: Pavia - p. 303 309; 313 314 Schornick http:/classweb.gmu.edu/jschorni/chem318

  • 12 Pages friedelcraftsakylation
    Friedelcraftsakylation

    School: George Mason

    FriedelCraftsAlkylation Purpose Preparationof4,4ditertbutylbiphenylusingthe FriedelCraftsalkylationofBiphenylthrough ElectrophilicsubstitutionofaLewisBase(tButyl Chloride(Haloalkane)inthepresenceofFerric ChlorideactingasaLewisAcid References: Website:http

  • 12 Pages dibenzalacetone
    Dibenzalacetone

    School: George Mason

    SynthesisofDibenzalacetone SynthesisofDibenzalacetoneMixedAldolCondensation (ClaisenSchmidt)reactionbetweenAcetoneand Benzaldehydeinthepresenceof95%Ethanoland20% SodiumHydroxide References: Pavia 04/22/12 Slayden p.77 Schornick http:/classweb.gmu.edu/jsch

  • 29 Pages brominationtoluene
    Brominationtoluene

    School: George Mason

    ElectrophilicAromaticSubstitution (BrominationofToluene) Demonstrationoftheeffectofamonosubstitutedelectron donargroup(ringactivator)onsubsequentsubstitutionof othergroupsontheBenzenering References 04/22/12 SlaydenLabManual p.7576 Website:http:/classweb

  • 31 Pages aldehydes&ketones
    Aldehydes&ketones

    School: George Mason

    Aldehydes&KetonesClassificationTests TheuseofChemicalClassificationTests, SelectedPhysicalProperties,NMR,andIRto IdentifyanUnknownAldehydeorKetone References: Pavia 04/22/12 Slayden p.7376 WebNotes http:/classweb.gmu.edu/jschorni/chem318 p.491496 1 Aldehy

  • 17 Pages acetanilide
    Acetanilide

    School: George Mason

    SynthesisofAcetanilide SynthesisofAcetanilideNucleophilicAcyl Substitution(addition/elimination)reaction betweenAnilineandAceticAnhydride References Pavia Schornick http:/classweb.gmu.edu/jschorni/chem318 04/22/12 p.6568 1 SynthesisofAcetanilide Overvie

  • 3 Pages Chem318handout
    Chem318handout

    School: George Mason

    Course: Organic Chemistry Lab II

    Organic Chemistry Lab (Chem 318) Organic Chemistry Lecture (Chem 314) is a Pre- or Co-requisite for this Course Instructor: Assistant Professor Barney Bishop Contact Information Office: Bull Run Hall, room 328C e-mail: bbishop1@gmu.edu Telephone: 703

  • 22 Pages aldehydes&ketones
    Aldehydes&ketones

    School: George Mason

    Course: Organic Chemistry Lab II

    Aldehydes & Ketones Classification Tests Overview Identification of Aldehyde/Ketone Unknown Liquid Unknown Purification & B.P. (Simple Distillation) Solid Unknown Melting Point Solubility Relative to Water & Sulfuric Acid Density Relative to W

  • 12 Pages acetanilide
    Acetanilide

    School: George Mason

    Course: Organic Chemistry Lab II

    Synthesis of Acetanilide Overview Synthesis of Acetanilide Nucleophilic Acyl Substitution (addition / elimination) reaction between Aniline and Acetic Anhydride Determine Mass, Moles, Molar Ratio, Limiting Reagent, Theoretical Yield Recrystallize

  • 19 Pages NMRspectroscopy
    NMRspectroscopy

    School: George Mason

    SpectroscopyExperiment(NMR) DeterminationoftheIdentityofanunknown organiccompoundusingselectedphysical properties,InfraredSpectroscopy,andNMR Spectroscopy UnknownList:pp.126127inSlaydenLabManual References Slayden,etal.pp.5960 Pavia,etal. Schornick 04/

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