Spec3(aromaticscarbonyls) - IR Spectrum(liquid lm 4000 3000...

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Unformatted text preview: IR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 v (cm‘) 125/127 Mass Spectrum % of base peak M+' 160/162l164 4o 80 120 160 200 240 280 m / e 13c NMR Spectrum (50.0 MHz, CDCI3 solution) proton decoupled 1H NMR Spectrum (200 MHz. coca3 solution) expansion lR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 0-0 V (cm'1 ) Mass Spectrum absorbanoe UV spectrum 104.1 mg] 10 mls i path length: 0.2 cm solvent : ethanol % of base peak 40 80 120 1 60 200 240 280 200 250 300 35. 0 ' m / a 7» (nm) ‘ 13C NMR Spectrum ( 20.0 MHz. CDCZl3 solution) proton decoupled 200 160 120 80 40 o 5 (pprriu 1H NMR Spectrum ‘5 (100 MHz. CDC!3 solution) 1 TMS 1 0 9 8 7 6 5 4 3 2 1 O S Innn n IR Spectrum (nujol mull) 4000 3000 1 V (cm' ) M+‘ 234l236l238 absorbence UV spectrum a 15.07'mg/10ml b 0.302 rug/10ml path length : 0.5 cm solvent : ethanol 155/157 % of base peak 40 80 120 160 200 240 280 200 250 300 350 m / e 7» (nm) 13C NMR Spectrum (20.0 MHz, CDCI3 solution) proton decoupled 1H NMR Spectrum (100 MHz. CDCI3 solution) IR Spectrum (CHCI; solution) 4000 3000 2000 1 1600 1200 800 0-0 V (cm' ) UVspectrum 1.032 mgl10mls path length: 1.00am solvenl : cyclohexane % of base peak 40 80 120 1 60 200 240 280 200 250 300 «3 50 m / e A. (nm) off-resonance decoupled 13c NMR Spectrum (20.0 MHz. (:DCI3 solution) TMS proton decoupled 200 160 120 80 40 o 6 (pp? 1) 1H NMR Spectrum 9 (100 MHz. CDCl3 solution) ’——/—— TNS 1o 9 8 7 6 5 4 3 2 1 c 8 (ppm) IR Spectrum (liquid film) 3000 2000 1 1600 1200 800 V (cm' ) 120 160 m/e 13c NMR Spectrum (50.0 MHz. CDCI3 solution) proton decoupled 200 160 1 20 80 1H NMR Spectrum (600 MHz, CDCI3 solution) UV Spectrum km 262 nm (Iogms 2.5) 40 solvent : ethanol o 5<ppmi ...
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  • Fall '09
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