Period_7

Period_7 - Period 7 Reaction 1 O (1) Diss in aq. HCl Ph NH2...

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Period 7 Reaction 1 Ph NH 2 O N H CH 3 Ph (1) Diss in aq. HCl (2) Ac 2 O/aq NaOAc Mechanism Ph NH 2 HC l Ph N H H H HOAc Ph NH 2 Ac 2 O /aq NaOAc O O OH O O N H 2 OH Ph O N CH 3 Ph H H O N H CH 3 Ph HOAc -H + Reaction 2 O N H CH 3 HNO 3 /H 2 SO 4 O N H CH 3 O 2 N Mechanism O N H CH 3 N + - O O OH H N + O O OH H N + O HO HO O N H CH 3 H N + O HO O N H CH 3 H H B N + O O O N H CH 3 H B N + O O O N H CH 3 Reaction 3 O N H CH 3 O 2 N 1. Reflux with HCl/H 2 O 2. Treat with aq NH 3 NH 2 O 2 N Mechanism O N H CH 3 R R= O 2 N H O N H CH 3 R OH 2 O N H CH 3 R H OH H O CH 3 H HO O N H 2 CH 3 R H OH NH 2 R +
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Procedure 50 mL 2.3 mL aniline 25 mL H 2 O 4.0 mL 20%HCl In a separate vessel, put 4.0g NaOAc. Cork and let the mixture stand a week. If it has suspended material. If the solution is deeper colored than lemon yellow. Keep the filtrate. Add decolorizing charcoal . The volume equals a large pea Wash it with 5 mL water. 125
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This lab report was uploaded on 10/08/2007 for the course CHEM 322BL taught by Professor Singer during the Spring '07 term at USC.

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Period_7 - Period 7 Reaction 1 O (1) Diss in aq. HCl Ph NH2...

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