C2510_Baeyer_Villager_S_2009 - Chemistry 2510 Introduction...

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Chemistry 2510 Introduction to Experimental Organic Chemistry Spring 2009 Experiment #7 Solvent-free Baeyer-Villager Oxidation Laboratory Notebook : You need to summarize your experimental plan in your lab notebook. Be sure to include a table of all reagents and compounds that will be used in this experiment. Laboratory Observations: Be sure to record any observations during the laboratory. You must record exactly how much of the starting materials you started with and the weight of the isolated product. Results and Conclusions : Calculate a % yield for the reaction, obtain an IR spectrum of the product and determine the melting point of the product. Relevant Reading: Technique 1, Crystallization, pp 23-38, Technique 2, Melting Points, pp 39-48, Technique 3, Extraction, pp 49-70, Technique 4, Drying Organic Solutions, pp 71-75, Technique 14, Carrying Out Typical Reactions, pp 153-162, Technique 15, IR Spectroscopy, pp 163-178. Background:
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This note was uploaded on 04/01/2009 for the course CHEM orgo lab taught by Professor Thm during the Spring '09 term at Cornell.

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C2510_Baeyer_Villager_S_2009 - Chemistry 2510 Introduction...

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