NMR-Slides1 - Ckae‘ter |'MUclear Wfingtt'g Reaoruqma 5 cc” F0569 A Mtjne'h'c Nude(5,Na‘t’urt a" NMR Abaarp‘f'una A magma-H

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Unformatted text preview: Ckae‘ter |\'MUclear Wfingtt'g Reaoruqma 5: cc”! F0569 A. Mtjne'h'c Nude}. (5,Na‘t’urt. a": NMR Abaarp‘f'una A. magma-H; NULlCL . '— \‘1cg*£fid a #- Mfioflc+ it. Flé' l‘ . Clause.» 5m; Manta; C "I-I, mark." F) halal a-kkers 1'9 bah-we. l" I“. aflhuiv mooth Twig-4r N‘H‘l‘ dub-I‘— T1" Nude“ 4,064.: + _ 'd no! It 5:94 .‘WIYWj “‘W” ‘1'“ *fl'hd Lia. «WERE; M, in.” "man a Nuclear 36w bdrm Ha I ———Jp;u.: Align-:6. Law-.131: ptcld IT? .. Th; 51-h #4 5E «kph-£4 0N “(tug-6k of «Hg; Applied Full, ('41:). I» '1' 1- ; 6.0an H [‘3 H3O 9g,st $ A E "' 1'9 -}¢ '3' - a: w $4; m m :1. MWW a. m“; a“ awn.) "*3? £14 Ln", " then-t; a}: 9»: M5), :5, H, fifififitrh‘EG-J Fan..-k.5 w“ a?» firms-3h . Seiau thy-mitt «II-1M Flt“ B.Nn.‘l'urc. o‘F NMR. abdarp-Hons - ~19ch [a malgwlts aft- Jurrmdu, by . decrka clam” ' APPl‘Icg'l-f...) O£ Hg => fi‘ec'h‘wl J‘a;fll 1:) I Llfl‘i - Th1. muclu Std}; tau-J e'Flccurwt mgamc'h'c. I Fliul Ht“. first i; “at ivm a»; mg ‘CWUJ Hag-4: :2 1-}; l-\r%__wk . m «finch all? J u. PFtrcart (Jyhnt‘t’fi “My unnamed-wt) wuei. kw; dx-FFcrmt =? JJF'FCMAV Hwy: =)JvFF¢M Hitach =) Eack “m” A? kyéraaea: 3.1m .. mam peak ' a HUN “Ann, 1“ \{IMJH gnu-é d6 “fwd?— 5m 4m EDD EDD 10”] [II II: I_I_|'_I"'|'| 'I |'| I | ' | | | | | | I | | | i I | I I'll I II (3an __ I ___II ' 5 L_ _._.__..!_..|_:_5__.| .| . | | | ._|__J . ' ' ' I |_|_- ' I | [5.0 in {H} FL” 4.0 31'] 2.0 ‘I.EI U PPM [fr] EDD 413C! EDD 200 100 0 H2 I—I—rI—rI—Ii—Ifi—I'I "' | ' | | ' I | ' | I | | i I I I ' I' ' I': 3 | I' ' 'I""I_'I I_I_|'_I_ I U _ II :41 Lune} 11 a gHDé-o (“I-1J w J_|_|_IJ_I__LJJ____1.I.I. |.|I..||'.|I.I|.|. [5.0 7H} 5.0 5.0 4.5- 311 2.4;! " .iu'“ " 0 PPM (.5; . FIGURE 11.1 Pretnn magnetic resonance spectra of iedemethane and methyl acetate. In. 393] Cupy‘rlghtfll 1934 by D. G. Heath and Germany. THflNSPAHENCY 33 HM LJHWJ 0 mafia: Ending Tffiafliflmi'fiegr ' 50 MIN: Lur- H .5" M’Ha GM “3c =7 Tm... JCIJQ, 1:6 N’MK £1 5'9“) "'0 3-H" "Caflflflf dié'l'ln’Jfll-SK bah):ch rapds, MDUITJ qwfibm}. ! “Cami bl. United. '30 McMult CONFDTML+IMI eka~5e. (0-. Chem; «.1 Skx'F-H :9 fit ckmlm slet 0F c. pun '3 Wt ‘@:€&?I.o~ #9 W"? pang fin 4,, (Vme .. " The. Units 9'5 ckzm{cu.$ SKI'F'E an I $g£l$llvq| a flu. #- 95 pdthcrm1l1ioA I the. radio crcfiuwcr wed, (elm-+1.41. "l'a tarmac-rm! Shel-um (Tm) CH; great: I wk“, 95a; 4%: Fla-hp 7, Frqam, .f- Jam-gig 4"?”“5 m9 ‘HW Gppliat WEI-5t: FrCfJWQYi ‘mfi‘t S 55 wdvefwmdw't' 9; ram Fragmwp 1 i o Figure15.5 a HCDNHI and ArOII-I .BFQUH RCI-IC‘I F2 'I'U Figure 15.5 F. CHE—{H3 CHI—CI CHg—UL'H; Page 696 f: Mb 5 3.06 'n 3.24 ‘3' CHE—CHa—U—H CHg—C—D—H Page '59? a 4.5 310-43 Sui-ye". Organic Chemistry @1999 University Stlerice Books. All rights reserved. HDH and RNH: (15.4] {15.51 15.1 EDD 400 EDD EDD ‘IEID {I Hz 8.0 10 5.13 5.0 4.0 3D 2.0 1.0 D F‘F‘Mfi] SUD 0U BUD HUD 101} U HZ _T_l—|_|_|_|_|_|_|_I'"]"'I I I 'r I I I I' I"|"|_|_|_|_I_|_I_I_["rl_|_l_|_|_|_l_l_l_'lml | I | | I I 1 I | JJ.I I.|J_I_I_IJ_I_I_I_IJ_LI.I_ 0.0 10 0.0 5.0 4.0 ' 0.0 2.0 1.0 0 FPMIIII . FIGURE 11.? Pr0t00 magnetic remnance spectra for 0y0I0h0X000 and t0luene. [0. 40?} oupyrighm 1004 1.1:.- 0. 0. Hufllll and {:nmlmrw TF‘lJ-‘I NS PAH ENEY 35 59in: -* 59in: SMJHMJ U H.‘ Hb HIL'; tun-c. e7li'ldfl’fm" C\“C- é-Hb Hy, a.“ ¢1Hnfihh~¥ ‘ I H“ H5 ‘4‘ +- p... m inc-Fng fi‘mli HEM! Hat-E 1H1??? “[1 E» Hwy” ,4- LM ._. 4.. 4.; 1‘. Mfiég; Hi! ‘ 3 : 3 - I 1' ,M1 H? ‘ \ 9 My? LN, * I 1-; M1” TN N “.4. 1~1~ yr 44, what “.5 “In “kg-t Hh'; “ace vm h02MI¢1MZ¢EH FEES Fa ES: .0 .u .fl Em... EFETES 5qu .3 .mcmEmEUEuE; #59 Earn..QO mucmgmm. unmcmmE :EEu m. :. mung“. “22¢; a 3 am. 3 3. an 3 E E NI 0 on: com Dom Dov com 500 400 000 200 I00 0 Hz . B]. O I CHICHCH. 8.0 TD 6.0 5.0 4.0 3.0 2.0 PPMIfli] EDD 411E! _ 300 200 100 1] Hz I I 'I I" | I—I"'I I I— t: HHCHchEBI' |_I_I .l IJ_I_I_I_I_|_I_L_I_I_|_I_I_I_I_|_I_I_I_I_|_I_I. I I_| 0.0 0.0 0.0 5.0 40 3.0 2.0 000003; 113 Lil .FIGURE 11.1? Pr010n magnetic I'E'SUFIEFICE spectra of 2—br0mnprnpane and 1—br0mopr0pane. (p. 418) Cupjnlglllfill 1954 by D. G. Heulh Imd Cunpuny. THANSPA HENCY 33 '_'_'_J_"“_‘_l_h'_'_"'|—"'_'_I—"*—'_I’“ ‘_‘—|"_'_'_I_'_""_|_'_'T—'“r—'—'_'_| '—I—* acc JED we 14:} 12c 1'30 ac ac are ac I PPM r'GUFEE 11.29 Free-jnducticn decay,»r data and prctcn-deccupfed and cfi-reacnance prc’rnn- -ccupled carbon—13 nuclear magnetic resonance spectra icr 4—methyl~2—penrancne. recorded an a Bruker WM-BBU nuclear magnetic resonance apectrcmeter. (p. 43D} THANEF‘AHENGY 4?. ‘ C-cpwlghlfl 1549-1 by 13-. C. I-Jcarh anri fiurnpany, ...
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This note was uploaded on 05/18/2008 for the course CHEM 320A taught by Professor Lopez during the Spring '08 term at CSU Long Beach.

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NMR-Slides1 - Ckae‘ter |'MUclear Wfingtt'g Reaoruqma 5 cc” F0569 A Mtjne'h'c Nude(5,Na‘t’urt a" NMR Abaarp‘f'una A magma-H

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