12Expt.15-NMRreportguidelines

12Expt.15-NMRreportguidelines - Experiment #15: Nuclear...

Info iconThis preview shows pages 1–2. Sign up to view the full content.

View Full Document Right Arrow Icon
CHEM 14CL Summer 08 Experiment #15: Nuclear Magnetic Resonance Spectroscopy Pre-lab Report MUST be written inside the lab notebook Pre-lab Report Guidelines (2) Procedure in Flowchart Format & Reference (3) Pre-lab study questions Complete ALL the study questions on page 146 of your lab manual (MUST SHOW ALL YOUR REASONINGS IN ORDER TO RECIEVE FULL CREDIT) Note: There are TWO signals around 130ppm in spectrum 1 on page 138 of the lab manual. Also ignore any signal that appears at 0ppm. Use the DEPT table on page 137 (or the one on the lecture guide) when answering question #3 of the study question. Remember that in DEPT spectroscopy, carbons with no hydrogen attached give no signals on the DEPT spectra.
Background image of page 1

Info iconThis preview has intentionally blurred sections. Sign up to view the full version.

View Full DocumentRight Arrow Icon
CHEM 14CL Summer 08
Background image of page 2
This is the end of the preview. Sign up to access the rest of the document.

Unformatted text preview: Experiment #15: Nuclear Magnetic Resonance Spectroscopy Post-lab (This post-lab is due at the END of the NMR Spectroscopy Workshop) Turn in ONE Post-lab Per Group Your Post-lab is the COMPLETED NMR WORKSHEETS (will be provided in the lab). (1) Write the names of your group members on EACH page of the worksheet. (2) Answer questions (1) - (3) in lab (see page 139) Note: for question #3, your group needs to PREDICT the 13 C, DEPT 45 & 90 spectra for EACH of the isomer. (3) Answer questions (4) - (6) in the computer lab (see page 139 & 140) Note: for question #6, your group need to COMPARE your predicted 13 C, DEPT 45 & 90 spectra with the computer generated spectra for EACH of the isomer. Staples all the worksheets (if you take them apart during the lab period) and turn them in to your TA at the end of the lab period....
View Full Document

This note was uploaded on 08/27/2008 for the course CHEM 14CL taught by Professor Henary during the Summer '08 term at UCLA.

Page1 / 2

12Expt.15-NMRreportguidelines - Experiment #15: Nuclear...

This preview shows document pages 1 - 2. Sign up to view the full document.

View Full Document Right Arrow Icon
Ask a homework question - tutors are online