C2510_Distillation_2008

C2510_Distillation_2008 - Chemistry 2510 Introduction to...

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Chemistry 2510 Introduction to Experimental Organic Chemistry Fall 2008 Experiment #3 Distillation Laboratory Notebook : You need to summarize your experimental plan in your lab notebook. Be sure to include a table of all reagents and compounds that will be used in this experiment. Laboratory Observations: Be sure to record any observations during the laboratory. You must record exactly how much of the starting materials you started with and the weight of the isolated product. Results and Conclusions : You should plot a graph of distillate volume versus temperature. You should determine, upon consultation with your peers, which method of distillation is most effective at separating components for each of the mixtures (taking into account purity, yield, and efficiency). Relevant Reading: Technique 5, Simple Distillation, pp 77—92 and Technique 6, Fractional Distillation, pp 93-97. Safety Considerations: The solvents you will be working with are flammable and should only be heated using the assigned apparatus. Your apparatus should be approved by your TA before heating is begun.
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