Lab Report 10- E1 Elimination Reaction.docx

Lab Report 10- E1 Elimination Reaction.docx - Ty Sides Lab...

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Ty Sides Lab Partner- Danae Parman, Lauren Garcia 6/6/17, CHEM 3105-303 TA- Nanda Katakam Experiment 10: The E1 Elimination Reaction: Dehydration of Cyclohexanol to Yield Cyclohexene Purpose The purpose of the experiment is to carry out an E1 elimination reaction. Another purpose of this reaction is isolate and characterize the product of the reaction. Reaction and Physical Properties Table Compound MW Amount mmol bp( C) d Cyclohexanol 100.6 8.0mL 7.7 160.8 0.96 Concd sulfuric acid 98.08 5-8 drops --- --- --- Concd phosphoric acid 98.00 2.5mL --- --- --- Br 2 159.808 --- --- --- --- CCl 4 153.81 --- -- --- --- CH 2 Cl 4 85.07 --- --- --- --- Safety The following is data obtained from the safety and documentation information made available at . Cyclohexanol (Irritant) Risk Statement: Harmful if inhaled, Harmful if swallowed, Causes skin irritation, May cause respiratory irritation Safety Statement: Avoid breathing dust/fume/gas/mist/vapours/spray. Sulfuric acid (Corrosive) Risk Statement: May be corrosive to metals, Causes severe skin burns and eye damage Safety Statement: Do not breathe dust/fume/gas/mist/vapours/spray, Wear protective gloves/protective clothing/eye protection/face protection, IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower, IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing and Immediately call a POISON CENTER or doctor/physician, IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing Phosphoric acid (Corrosive) Risk Statement: May be corrosive to metals, Causes severe skin burns and eye damage
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Safety Statement: Wear protective gloves/protective clothing/eye protection/face protection, IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower, IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing and Immediately call a POISON CENTER or doctor/physician, IF IN EYES: Rinse cautiously with water for several minutes. Remove contact
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