Lab Report 3- Hydroboration Oxidation of an Alkene- 1 octene.docx

Lab Report 3- Hydroboration Oxidation of an Alkene- 1 octene.docx

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1-OCTENE 3 Ty Sides Lab partner- Danae Parman 7/16/17, 3106-302 Umut Ozuguzel, Arpita Singh Experiment 3: Hydroboration-Oxidation of an Alkene: Octanol Purpose The purpose of this experiment is to demonstrate the conditions required for a hydroboration reaction to occur on an unsaturated hydrocarbon. This experiment also demonstrates the ease of preparing alcohols from the alkylborane intermediates. Reaction and Physical Properties Table Compound MW Amount mmol bp ( C) d N D 1-Octene 112.22 420 L 2.68 121 0.72 1.4087 Borane THF (1M) --- 2.0mL 2.00 --- --- --- Sodium hydroxide (3M) 40.00 600 L --- --- --- --- Hydrogen peroxide (30%) 34.01 600 L --- --- --- --- Safety 1-octene(Flammable, Health Hazard, Environmental Hazard) Risk Statement: Highly Flammable liquid and vapour, May be fatal if swallowed and enters airways, Very toxic to aquatic life with long lasting effects Safety Statement: Keep away from heat/sparks/open flames/hot surfaces. — No smoking, Avoid release to the environment, IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician, Do NOT induce vomiting, Dispose of contents/container to..… 1M Borane THF (Flammable, Corrosive, Irritant, Health Hazard) Risk Statements: Highly Flammable liquid and vapour, In contact with water releases flammable gases which may ignite spontaneously, Harmful if swallowed, Causes skin irritation, Causes serious eye damage, May cause respiratory irritation, Suspected of causing cancer Safety Statement: Keep away from heat/sparks/open flames/hot surfaces. — No smoking, Handle under inert gas. Protect from moisture, Wear protective gloves/protective clothing/eye protection/face protection, In case of fire: Use … for extinction, Store in a dry place, Store in a closed container, Store in a well-ventilated place. Keep cool.
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