Lab Report 4- Diels-Alder Reaction.docx

Lab Report 4- Diels-Alder Reaction.docx - Ty Sides Lab...

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Ty Sides Lab partner- Danae Parman 7/18/17, 3106-302 Umut Ozuguzel, Arpita Singh Experiment 4: Diels-Alder Reaction: 9,10-Dihydroanthracene-9,10- , -succinic Acid Anhydride Purpose The purpose of the experiment is to demonstrate the role of an aromatic ring system as the diene substrate in an addition reaction. This reaction, specifically, exemplifies the 1,4 addition by an acitivated alkene dienophile to make the products, adducts. Reaction and Physical Properties Table Compound MW Amount mmol mp ( C) bp ( C) Anthacene 178.24 80mg 0.44 216 --- Maleic anhydride 98.06 40mg 0.40 60 --- Xylenes --- 1.0mL --- --- 137-140 9,10- Dihydroanthracene -9,10- , -succinic Acid Anhydride 276 --- --- 261-262 --- Safety Anthracene (Irritant, Environmental Hazard) Risk Statement: Causes skin irritation, Causes serious eye irritation, May cause respiratory irritation, Very toxic to aquatic life with long lasting effects Safety Statement: Avoid breathing dust/fume/gas/mist/vapours/spray, Avoid release to the environment, IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing, Dispose of contents/container to.
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