AnsRev22 - Review for Chap 22 O Br2 HOAc O O Br O Br2...

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Review for Chap 22 O O OH O OH O O CH 2 Br 2 HOAc Br 2 NaOH/H 2 O Br 2 HOAc PBr 3 Br 2 , HBr 1. PCl 3 , Cl 2 , HCl 2. H 2 O H 2 O O OH O OEt O O CH 2 LDA (1 eq) LDA (1 eq) LDA (1 eq) CH 3 CH 2 Br CH 3 CH 2 Br O O D 2 O, D + 1. LDA 2. D 2 O OH OO heat HO OH heat OH O heat (< 300C) O Br O Br O - O + CHBr 3 Br 2 NaOH/H 2 O O Br Br O CHBr OH O CHBr OH O Cl CH 2 - O O CH 2 CH 3 O - Li + O CH 2 + HN OEt O O D O D D 3 O eventually O + CO 2 HO O + CO 2 no reaction
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Useful synthetic recipe: EtO OEt OO OEt NaOEt EtBr H + , H 2 O heat NaOEt EtBr H + , H 2 O heat MeO OMe NaOMe
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AnsRev22 - Review for Chap 22 O Br2 HOAc O O Br O Br2...

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