Postlab5 - filtration I forgot to wet the filter paper to...

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Dong Hyun Suh Mr. Erdei CHE2204 March 16, 2009 Post-Laboratory Report Hypochlorite Oxidation of Methyl Ketones by the Halofom Reaction: Bezonia Acid and p-Methoxybenzoic Acid Data: Product: 0.019g Published Melting point: 181-186 C Experimental Melting point : 187-190 C Calculations: Theoretical yield calculation Percent yield calculation Results/Conclusion: Through the experiment, I lost much of the product by making a mistake during the
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Unformatted text preview: filtration. I forgot to wet the filter paper to be placed properly. This was a very good experience in preparation for the final practical. I found the melting point of the final product; it was much higher than the published melting point. This is most likely because of not dried product, and the remaining moisture caused a higher melting point than expected....
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