Postlab7 - intermediate compound to have the final product...

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Dong Hyun Suh Mr. Erdei CHE2204 March 30, 2009 Post-Laboratory Report Imide Synthesis: Preparation of N-phenylmaleimide Data/observation: Start material: 0.131 g Product: 0.210 g Published Melting point: 162-163 C Experimental Melting point: 180 C Calculations: Theoretical yield Percent yield Results/Conclusion: For this experiment, everyone was told to double the amount of reagent. I think this was a wise choice since this reaction is happening in microscale. We had to make the
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Unformatted text preview: intermediate compound to have the final product. I ended up with fair amount of product, but I found out that a significant amount of product was washed away during filtration. Also, the melting point was much higher than expected, and the reason could have been the moisture left in the compound....
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