chapter6.pdf - SECTION 600 Pesticide Analytical Manual Vol...

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Transmittal No. 96-E1 (9/96) Form FDA 2905a (6/92) 600–1 SECTION 600 Pesticide Analytical Manual Vol. I Table of Contents page date 601: General Information 601 A: Principles 601-1 1/94 601 B: Modes of Operation 601-2 1/94 Liquid-Solid Chromatography 601-2 1/94 Liquid-Liquid Chromatography 601-3 1/94 Bonded Phase Chromatography 601-3 1/94 Ion Exchange Chromatography 601-4 1/94 Size Exclusion Chromatography 601-4 1/94 601 C: Instrumentation and Apparatus 601-5 1/94 Basic Components 601-5 1/94 HPLC System Plumbing 601-7 1/94 601 D: Solvents and Reagents 601-10 1/94 Potential Problems 601-10 1/94 Specific Solvents 601-12 1/94 Chapter 1 Regulatory Operations Chapter 2 General Analytical Operations and Information Chapter 3 Multiclass MRMs Chapter 5 GLC Chapter 4 Selective MRMs Chapter 6 HPLC
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Transmittal No. 96-E1 (9/96) Form FDA 2905a (6/92) 600–2 Pesticide Analytical Manual Vol. I SECTION 600 page date Reagent Blanks 601-14 1/94 Safety Precautions 601-14 1/94 601 E: Sample Preparation 601-14 1/94 Sample Cleanup 601-14 1/94 Sample Filtration 601-14 1/94 Sample Solvent Degassing 601-15 1/94 Choice of Sample Solvent 601-15 1/94 601 F: Reference Standards 601-15 1/94 Stock Solutions 601-15 1/94 Working Standard Solutions 601-16 1/94 Storage 601-16 1/94 References 601-16 1/94 602: Columns 602 A: Column Selection 602-1 1/94 602 B: Analytical Columns 602-1 1/94 Liquid-Solid Chromatography 602-2 1/94 Bonded Phases 602-2 1/94 Ion Exchange 602-3 1/94 Ion Pair 602-4 1/94 Size Exclusion 602-4 1/94 602 C: Column Evaluation 602-5 1/94 602 D: Column Specifications 602-6 1/94 602 E: Analytical Column Protection 602-8 1/94 Filters 602-8 1/94 Precolumns 602-9 1/94 Guard Columns 602-9 1/94 602 F: Column Maintenance and Troubleshooting 602-9 1/94 Column Care 602-9 1/94 Column Evaluation by Injection of 602-10 1/94 Test Mixtures Column Storage 602-11 1/94 Column Regeneration 602-11 1/94 References 602-12 1/94 603: Mobile Phase Selection, Preparation, and Delivery 603 A: Mobile Phase Selection 603-1 1/94 Normal Phase Chromatography 603-1 1/94 Reverse Phase Chromatography 603-3 1/94 Ion Exchange Chromatography 603-4 1/94 Ion Pair Chromatography 603-5 1/94 Size Exclusion Chromatography 603-5 1/94 Gradient Elution in HPLC 603-5 1/94 603 B: Mobile Phase Preparation 603-6 1/94 Filtering Solvents 603-6 1/94 Degassing Solvents 603-6 1/94
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Transmittal No. 96-E1 (9/96) Form FDA 2905a (6/92) 600–3 SECTION 600 Pesticide Analytical Manual Vol. I page date Preparation of Multisolvent Mobile Phases 603-7 1/94 Solvent Reservoirs 603-7 1/94 603 C: Mobile Phase Delivery Systems 603-8 1/94 Pumps 603-8 1/94 Gradient Programming Systems 603-10 1/94 603 D: Maintenance and Troubleshooting 603-10 1/94 Problems with Pumps 603-10 1/94 References 603-13 1/94 604: Injection Systems 604 A: Injection Valves 604-1 1/94 604 B: Automatic Injectors 604-3 1/94 604 C: Operation, Maintenance, Troubleshooting, 604-3 1/94 and Repair of Injection Valves References 604-4 1/94 605: Detectors 605 A: UV/VIS Absorbance Detectors 605-2 1/94 Fixed Wavelength UV Detectors 605-3 1/94 Variable Wavelength UV Detectors 605-4 1/94 Solvents 605-4 1/94 Performance Characteristics 605-4 1/94 Multichannel or Photodiode Array Detectors 605-5 1/94 Applications 605-5 1/94 Problems, Maintenance, and 605-5 1/94 Troubleshooting 605 B: Fluorescence Detectors 605-6 1/94 Detector Design 605-6 1/94
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