C2510_Green_Oxidation_S_2009 - Chemistry 2510 Introduction...

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Unformatted text preview: Chemistry 2510 Introduction to Experimental Organic Chemistry Spring 2009 Experiment #12 “Green” Oxidation of Aromatic Aldehydes Laboratory Notebook : You need to summarize your experimental plan in your lab notebook. Be sure to include a table of all reagents and compounds that will be used in this experiment. Laboratory Observations: Be sure to record any observations during the laboratory. You must record exactly how much of the starting materials you started with and the weight of the isolated product. Results and Conclusions : Calculate a % yield for the reaction, obtain an IR spectrum of the product and determine the melting point of the product. Relevant Reading: Technique 1, Crystallization, pp 23-38, Technique 2, Melting Points, pp 39-48, Technique 14, Carrying Out Typical Reactions, pp 153-162,Technique 15, IR Spectroscopy, pp 163-178. Background: As students who have had laboratory experience in the general chemistry course and are currently partway through your organic laboratory course, you may have already noticed the stringent waste-disposal protocols...
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C2510_Green_Oxidation_S_2009 - Chemistry 2510 Introduction...

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