14CLlabscheduleF093

14CLlabscheduleF093 - CHEMISTRY 14CL LABORATORY...

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CHEMISTRY 14CL LABORATORY SCHEDULE (LAST DAY TO DROP THE CLASS: October 9 ) FALL 2009 SAFETY GLASSES AND LAB APRONS OR LAB COATS MUST BE WORN IN THE LABORATORY. FAILURE TO DO SO WILL RESULT IN DISMISSAL FROM THE LABORATORY Date Experiment 1 Videotape 2 Reading 3 Postlabs Due Date 4 9/24 – 9/25 1: Check-in, Pipet Calibration (1) Safety (#5805) M p. 2-27 NONE Use of a Pipet 9/29 – 10/7 8: pH titration of an amino acid (3) AJ p. 579-609; B p. 1034-1048 10/13 & 14 10/8 – 10/9 6: Aldol condensation (1) Melting Point M p.78-92 10/20 & 21 10/13 – 10/16 7a: Extraction of Caffeine (2) Extraction (#3132) M p.56 - 71 One postlab for 7a refer to due date shown below 10/20 – 10/21 7a: Analysis of Caffeine (1) M p. 152-162; p. 197-219; 284-296 10/29 & 30 10/22 – 10/23 7b: Spartan Infrared spectroscopy (1) IR (#3139) B Ch. 12 & 14 10/29 & 30 10/27 – 10/30 10: Oxidation of borneol to M p. 56-71; AJ p. 633-638; 11/5 & 6 Camphor (2) (handouts) M p. F95-F102 11/3 – 11/6 Titrimetric Analysis of Vitamin C (2) (Handouts) AJ p. 633-642; p. F 95-F 102 11/12&13 11/12 – 11/13 9: Distillation & Gas chromatography (1) Distillation (#3134) M p. 109-118 11/19 & 20 GC (#3134) M p. 163-177 11/17 – 11/18
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