Solutions_Manual_for_Organic_Chemistry_6th_Ed 284

Solutions_Manual_for_Organic_Chemistry_6th_Ed 284 - .' . ....

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13-13 (a) , . , ± ²³ ' 5. 1 1 ´µ¶ ·¸¹º 1 , ± , ± , ± J bc = l.4 H I I ± J bc = 1±4 H J-±² _ o c II a H C-OH \ / c=c fed / \ CH3CH2CH2 H b a = 8 ±²³´ (broad singLet, IH) b = 85µ (doubLet² c = 87·1 (muLtIpLet, d ¸ 8²µ² ³qUaRtet´ ²H) e ¸ 8 1·¹ ³sextetµ ²H) F = 80º9 ³t¶p·et, »H) (b¸ The v¹NyL proton at 8 7³ 1 Is H e ; ¹t Is coUp·ed wIth HB and Hd, witH tWo diFFerenº CoupLi»g conStants, J B e and JE d ' respect¹veLy± The va·ue of j B e can be measured Most preciseLy Fro¼ ºHE sigNa½ for
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