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Unformatted text preview: of the Celite. Place the Hirsch funnel atop a filter flask which has been attached to an aspirator. With the aspirator turned on, quickly pour the hot solution onto the Kimwipe atop the Celite. The colorless solution will be pulled into the filter flask. 5 Acetanilide should begin to form a white solid in the filter flask. To aid in crystallization, place the flask in an ice bath. If no crystals form after several minutes, transfer the liquid to a clean flask and reheat to boiling for a few minutes. Then, cool this flask. 6 Product is recovered by collecting the solid product on a Hirsch funnel. Allow the solid to fully dry by storing it in your lab drawer until the next lab period. Then, record the mass of the product and obtain it's melting point. health & safety notes Acetanilide is a toxic and an irritant. Avoid contact with your skin. H N CH 3 O acetanilide...
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This note was uploaded on 03/10/2010 for the course CHEM 241 taught by Professor Crouch during the Spring '08 term at Dickinson.
- Spring '08
- Organic chemistry