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Sample Lab Notebook Page - CH COzCI'la CHgof CHQCHa...

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Unformatted text preview: CH COzCI'la CHgof. CHQCHa CH (DC-HS SJ T OH ' H. + _§__+_) - ' . C5115 4' “a; .0 . 70 on OH _ >< We. WWW claim-1W mmol 7-0-0 mm| 11.0 nun-ml Catalytlt. C-q ”HOG CtJnri‘U'Ly 356 g. ' 2.70 mL O. ‘00 9 FN: ZIBDSINDI eq'uiv. Loo sq: I. ID at _ TY: H3623 L-Dimcthql "turtrdtc. was placed I'n CI drq 50mL round bottom flask and dissolved in 20 mL csl‘ benzene. A Stir bar was added and loo m9 of T90“ was added to “the Stirring st'dm 1.1- Dimc'thoxypropmu was added \ilu syrihge, Cl Dean-Stark trap and tum-Coded Cdflemcr ultra Q’f‘fixeé to fl: 9qu and 'khe m'Imurc um. heated at reflw Over “Edit. the. reactlbn mixture, was allowed. to Cool at rt- Ibc reactlbn mixture, was. ‘tmnSfm-ed to u Separatory funnel and HR. flask finses-l with approilmu‘tdq ZOmL 0‘? either which ms added bathe Sap-Funnd._[he. mixture. UJQS. washed 3): MW Saturated. quumus Na H103 and once uii’dw wfier. The. orgufixc \oqu- was transient ' 'to on Ericnmy'u- “qu and dried with Mu 50% flak—{d ““6 CDHW‘UQ’CRG *0 give. H.119 of q Viscous Venom liquid. Utsfldh‘oon produced 3.173 (86 9° xjidd) 0+ a pale. yellow “quid whose. NMR Spectrum is Consistent LUIIth ‘U‘nu't 01‘ the. dcm'red, product. dimz'thgl 2. 3-D“I350Prom""Ck'flft‘flr‘i‘tE ...
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