Exp 7 - Friedel-Crafts Acylation of Anisole Tyler Argent...

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Friedel-Crafts Acylation of Anisole 11/10/08 Tyler Argent Exp. 7 CH 237 Lehman, John W. Operational Organic Chemistry, (Exp. 37 p.292 in text) I. Pre-Lab: (Attached) II. Experiment Notes and Observations: (Refer to Pre-Lab) III. Results: Compound MW (g/mol) Amt. Used Moles Used Physical Constants Anisole 108.2 1.0 mL 0.01 mol Flammable, Irritant b.p.=155°C m.p=238°C d=0.996 g/mL Acetic Anhydride 102.1 1.0 mL 0.011 mol Corrosive b.p=140°C m.p.=-73°C d=1.082 g/mL Anhydrous Aluminum Chloride 133.3 2.93 g 0.022 mol m.p.=193°C Aqueous Sodium Chloride 58.4 5.0 mL Irritant Dichloromethane 84.9 10.0 mL 0.16 mol Toxic, Irritant b.p=40 m.p=-95 d=1.327 g/mL Ice 18.02 10.0 g o-Methoxyacetophenone 150.2 b.p=245°C d=1.090 g/mL m-Methoxyacetophenone 150.2 b.p=240°C d=1.034 g/mL p-Methoxyacetophenone 150.2 b.p=258°C m.p=39°C d=1.082 ¹ g/mL 3 M Sodium Hydroxide 40 5.0 mL
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Theoretical Yield: 10 mmol (.010 mol) X 150.2 g/mol = 1.50 g Acetylanisole Weight(crude) of product after rotovap: 0.36 g Recovered product after distillation: 0.35 g Percent Yield: 0.35 g/ 1.50 g X 100 = 23.3 % **Total product recovered is a result of adding individual results to three other lab partners solutions for the distillation process to achieve greater results** Boiling Range: 130C- 135C **
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Exp 7 - Friedel-Crafts Acylation of Anisole Tyler Argent...

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