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Unformatted text preview: separatory funnel. 30 ml of HCl was then added and the funnel was shaken. After allowing the layers to settle, the pH of the top layer was tested. The top layer should be acidic. Two flasks were labeled. One labeled “Aspirin & Phenacetin” for the bottom layer and the other “Caffeine” for the top layer. Draw off each layer into the appropriate flask. O C H 3 NH CH 3 O OH O O CH 3 O N N N N C H 3 O O CH 3 CH 3...
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This note was uploaded on 05/04/2010 for the course CHEM 3361 LAB taught by Professor Tapu during the Spring '08 term at Kennesaw.
- Spring '08