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Lab 1 - Part 2 - Synthesis and Analysis of Iron Oxalate

Lab 1 - Part 2 - Synthesis and Analysis of Iron Oxalate -...

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CHEM 30AL Spring 2010 Experiment #11: Analysis of Iron oxalate Complex (PART 2) REDOX Titration Analysis of Iron Oxalate Complex by KMnO 4 IMPORTANT: Make sure that you follow the proper laboratory safety protocol (refer to the course syllabus) BEFORE going to the lab. You will be dismissed from the laboratory if you do not follow the proper safety protocol. Pre-lab Report Guidelines (i) Title (ii) Reference of procedures (iii) Introduction - summarize the goal(s) for this part of the experiment as well as any techniques ( including any synthetic; analytical and/or purification techniques ) that you will be using in achieving such goal(s). (iv) Procedures in flowchart format; you will do ONLY “ Titrimetric Analysis of Oxalate using KMnO 4 part, (refer to p. 101 under period 2 BUT NOT INCLUDING "Colorimetric Analysis of Iron". You will complete the flowchart for the colorimetric analysis in PART 3 of the pre-lab report) (v) MSDS information The following chemicals will require you to use the MSDS database on the Web: Potassium permanganate (0.05 to 0.15M)
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