Chem112C-LAB-S10-syllabus

Chem112C-LAB-S10-syllabus - C H E M I ST R Y 1 1 2 C L A B...

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Unformatted text preview: C H E M I ST R Y 1 1 2 C L A B O R A T O R Y E X P E R I M E N T S Sp r i n g 2 0 1 0 TEXTBOOKS M ic ro s c a le O rg a n ic L a b o ra to ry : a d a p te d f o r u s e in C h e m 1 1 2 C , U C R M a y o , P ik e , T ru m p e r J o h n W ile y & S o n s L A B O R A T O R Y I N ST R U C T O R P ro f e s s o r M ic h a e l P irru n g C h e m ic a l S c ie n c e s 1 , R o o m 4 4 8 ( 9 5 1 ) 8 2 7 - 2 7 2 2 , e - m a il: m ic h a e l.p ir r u n g @ u c r .e d u A C A D E M IC C O O R D IN A T O R D r. R o d n e y Je n k s S c ie n c e L a b o ra to rie s 1 , 1 0 3 ( 9 5 1 ) 8 2 7 - 3 1 4 3 ; e m a il: r o d n e y .je n k s @ u c r .e d u SP E C I A L L A B O R A T O R Y I N F O R M A T I O N (1 ) (2 ) It is n o t p o s s ib le to g e t a p a s s in g g ra d e f o r th e c o u rs e w ith o u t c o m p le tin g th e la b o ra to ry w ith a p a s s in g g ra d e . A c a d e m ic d is h o n e s ty in a n y fo r m w ill n o t b e to le ra te d in th is la b . In a d d itio n to th e s a n c tio n s im p o s e d o n la b o ra to ry g ra d e s , a ll s u c h in c id e n ts w ill b e re p o rte d to th e O f f ic e o f S tu d e n t C o n d u c t f o r a d m in is tra tiv e re v ie w . S tu d e n ts f o u n d to b e c h e a tin g w ill re c e iv e a z e ro g ra d e f o r th e e x p e rim e n t a n d m a y b e s u b je c t to d is m is s a l f ro m th e c la s s w ith a f a ilin g g ra d e . C h e a tin g in c lu d e s ( b u t is n o t lim ite d to ) tu rn in g in a re p o rt w ith o u t d o in g th e e x p e r i m e n t , i n t e r f e r i n g w i t h a n o t h e r s t u d e n t 's w o r k , r e m o v i n g c h e m i c a l s o r g l a s s w a r e f r o m t h e l a b o r a t o r y , o r p ro v id in g te s t q u e s tio n s o r a n s w e rs to o th e r s e c tio n s . A ll s tu d e n ts e n ro lle d in th is c la s s a re a ls o re s p o n s ib le f o r f a m ilia riz in g th e m s e lv e s w ith th e S tu d e n t C o d e o f C o n d u c t. T h e g e n e ra l ru le s a n d s tu d e n t rig h ts in th a t d o c u m e n t a p p ly to th is la b . A tte n d a n c e a t y o u r a s s ig n e d la b o ra to ry m e e tin g s is m a n d a to ry . If y o u m is s a la b o ra to ry y o u w ill n o t b e a b le to m a k e - u p th a t la b o ra to ry . F o r o n e a b s e n c e o n ly , w ith a v e rif ia b le m e d ic a l e x c u s e a c c e p te d b y D r. J e n k s , y o u r la b o ra to ry s c o re w ill b e p ro - ra te d . Y o u m u s t c o n ta c t D r. J e n k s b y te le p h o n e [ ( 9 5 1 ) 8 2 7 - 3 1 4 3 ] im m e d ia te ly u p o n le a rn in g y o u w ill m is s a la b , le a v e a p h o n e n u m b e r w h e re y o u c a n b e re a c h e d , a n d p ro v id e a m e d ic a l e x c u s e ( s ig n e d b y a lic e n s e d m e d ic a l d o c to r ( M .D .) ) to D r . J e n k s a s s o o n a s y o u r e tu r n to c a m p u s . Y o u r T A m a y n o t a lte r th is p o lic y . Lab Preparation Write-ups (Pre-Labs) are due at the beginning of the lab period in which the experiment is to be done. L a b o r a to r y R e p o r ts a re d u e a t th e b e g in n in g o f th e la b p e rio d f o llo w in g c o m p le tio n o f th e e x p e rim e n t. E n r o llm e n t q u e s tio n s c o n c e rn in g la b o ra to ry o r le c tu re m u s t b e d ire c te d to D r. J e n k s . N o te o n la b o r a to r y fe e s : Y o u r la b o ra to ry f e e w ill b e p a y in g f o r c h e m ic a ls , g la s s w a re , h o tp la te s , a n d o th e r a llo w a b le te a c h in g ite m s a n d a p p a ra tu s . C e llu la r P h o n e s : F o r s a f e ty re a s o n s c e llu la r p h o n e s m a y n o t b e o p e ra te d in th e la b o ra to ry . M a k e c e rta in th a t y o u r p h o n e is in th e o f f p o s itio n b e f o re e n te rin g . C o u r s e w r itte n m a te r ia ls : A ll c o u rs e w ritte n m a te ria ls a re c o p y rig h te d a n d p ro v id e d to s tu d e n ts e n ro lle d in th is c la s s f o r th e ir e d u c a tio n a l u s e d u rin g th is te rm o n ly . P ro v id in g th e s e m a te ria ls d o e s n o t tra n s f e r c o p y rig h t. A n y c o p y in g , tra n s m is s io n to o th e r p a rtie s in e le c tro n ic o r o th e r f o rm s , o r o th e r u s e s o f th is m a te ria l w ith o u t e x p re s s w ritte n c o n s e n t is s tric tly p ro h ib ite d . S u c h a c ts w ill b e p u n is h e d b y a 0 s c o re f o r th e la b , in te r a lia . T h e O rg a n ic C h e m L a b S u rv iv a l M a n u a l: A S tu d e n t’s G u id e to T e c h n iq u e s Z u b ric k , 7 th e d itio n J o h n W ile y & S o n s L e c tu r e In str u c to r s P ro f e s s o r C h ris to p h e r S w itz e r P ro f e s s o r C a th a rin e L a rs e n (3 ) (4 ) (5 ) (6 ) (7 ) (8 ) (9 ) SC H E D U L E O F E X P E R I M E N T S - C H E M 1 1 2 C ( Sp r i n g 2 0 1 0 ) ( L a b o ra to ry s e c tio n s m e e t M o n d a y th ro u g h T h u rs d a y ) D ays 0 3 /2 9 - 0 4 /0 1 E x p e r im e n t L a b o r a t o r y S a f e t y & C h e c k - i n . Y o u M U ST m a k e s u r e t h a t y o u h a v e a l l o f t h e n e c e s s a r y l a b e q u i p m e n t a n d g la s s w a re in y o u r a s s ig n e d d ra w e r b e f o re y o u le a v e . R e a d L a b te x t, p p i- x iii, E 0 , Z u b ric k , p p 1 - 3 6 . S y n th e s is o f D ib e n z a la c e to n e ( 1 5 p ts ). p p E 4 - E 9 . R e a d M c M u rry , p p 8 7 8 - 8 8 3 . Z u b ric k , p p 8 7 - 9 2 ( m e ltin g p o in t), 1 2 1 - 1 2 6 ( re c ry s ta lliz a tio n ), 2 7 5 - 3 0 2 ( in f ra re d s p e c tro s c o p y ). Id e n tific a tio n o f C a rb o h y d ra te s b y C h e m ic a l T e s ts ( 2 0 p ts ). p p E 5 1 - E 5 6 . R e a d M c M u rry , p p 9 9 2 - 9 9 3 , 999-1001. Do prelab questions 1-5 on p E53 and E55 prior to coming to lab. Q u a lita tiv e Id e n tific a tio n o f O rg a n ic C o m p o u n d s (s o lu b ility , L u c a s te s t, c h ro m ic a n h y d rid e te s t) ( 1 5 p ts ). R e a d p p E 0 - E 2 a n d la b te x t, C h a p te r 1 0 , p p 7 0 2 -7 1 7 . Q u a lita tiv e I d e n tif ic a tio n o f O r g a n ic C o m p o u n d s ( H in s b e r g te s t, 2 ,4 - D in itr o p h e n y lh y d r a z in e te s t, B e n e d ic t’s te s t, T C IC A te s t) ( 1 5 p ts ). p p E 0 - E 2 . R e a d E 5 3 - E 5 4 , la b te x t p p 7 0 6 - 7 0 7 , 7 1 2 - 7 1 3 , a n d a h a n d o u t to b e p ro v id e d . I d e n t i f i c a t i o n o f G e n e r a l U n k n o w n s W e e k 1 ( 4 0 p t s /u n k n o w n ) . B e s u r e t o p r e p a r e p r i o r t o c o m i n g t o l a b a f lo w c h a rt s h o w in g th e s e q u e n c e o f o p e ra tio n s y o u w ill b e p e rf o rm in g . R e a d p p E 0 - E 2 a n d la b te x t, C h a p te r 1 0 . I d e n t i f i c a t i o n o f G e n e r a l U n k n o w n s W e e k 2 ( 4 0 p t s /u n k n o w n ) . B e s u r e t o p r e p a r e p r i o r t o c o m i n g t o l a b a f lo w c h a rt s h o w in g th e s e q u e n c e o f o p e ra tio n s y o u w ill b e p e rf o rm in g . I d e n t i f i c a t i o n o f G e n e r a l U n k n o w n s W e e k 3 ( 4 0 p t s /u n k n o w n ) . B e s u r e t o p r e p a r e p r i o r t o c o m i n g t o l a b a f lo w c h a rt s h o w in g th e s e q u e n c e o f o p e ra tio n s y o u w ill b e p e rf o rm in g . Nylon 66 (15 pts). pp E44-E50. Read McMurry, pp 1213. Do prelab questions 1-2 on p E44 prior to coming to lab. Do postlab question 1 on p E45 and questions 8-40, 8-42, 8-44 on p E48-49. Monday la b : a ls o c h e c k - o u t. M e m o ria l D a y - H o lid a y . Check-Out---Reports due. 0 4 /0 5 - 0 4 /0 8 0 4 /1 2 - 0 4 /1 5 0 4 /1 9 - 0 4 /2 2 0 4 /2 6 - 0 4 /2 9 0 5 /0 3 - 0 5 /0 6 0 5 /1 0 - 0 5 /1 3 0 5 /1 7 - 0 5 /2 0 0 5 /2 4 - 0 5 /2 7 0 5 /3 1 0 6 /0 1 - 0 6 /0 3 L a b o r a to r y is w o r th a to ta l o f 2 0 0 p o in ts . Im p o r ta n t In fo r m a tio n T A N a m e_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ L a b Ro o m _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ L a b T i m e _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ L o c k e r N um b e r _ _ _ _ _ _ _ _ _ _ _ _ L o c k e r C o m b i n a t i o n _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ...
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This note was uploaded on 08/15/2010 for the course BCH 100 taught by Professor Staff during the Spring '08 term at UC Riverside.

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