d_alder_procedure - Diels-Alder Reaction Reference: 1....

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Diels-Alder Reaction Reference : 1. Williamson, Macroscale and Microscale Organic Experiments , 5 th edition, Houghton Mifflin: New York, 2007, Experiment 48.1 Cracking of Dicyclopentadiene, p. 665, performed in batch for the class by instructor Experiment 48.2 (1/6 X macroscale) cis-Norbornene-5,6-endo-dicarboxylic Anhydride, p 669 2. *Click on: http://ocw.mit.edu/OcwWeb/Chemistry/5-301January--IAP-2004/StudyMaterials/index.htm to view a video clip demonstration of ‘R ecrystallization methodology, courtesy of the free and worldwide MIT OpenCourseWare website. You’ll need the RealPlayer application; free download at: http://www.real.com/dmm/realplayer/search? pcode=srchrv&ocode=search&cpath=ppcse&rsrc=gg_rp_X1realplayer&gclid=CJ3gw7ncv58CFQKbnAodpCl70 w ACKNOWLEDGEMENT: Dr. Jeffrey wishes to thank Dr. Nomura for the basis for this handout. Note to 2642L Students: This handout provides the basic information you’ll need to perform this experiment. However, you will need to do some pre-lab research for the properties, molar quantities, and theoretical yield of these reactants and product. You should include, at a minimum: Formula MW # moles b.p. m.p. density (liquids) You may find this information from any of the following sources: Material Safety Data Sheets (MSDSs); just ‘google’ the compound’s name Wikipedia Williamson (Library reserve) Other Library sources
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Materials: 1. dicyclopentadiene [77-73-6] (cyclopentadiene dimer); note: this material will be cracked to the monomer by the lab instructor (see Procedure below). 2. cyclopentadiene monomer 3.
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This note was uploaded on 11/06/2010 for the course CHEM 10258 taught by Professor Dr.doodoohead during the Spring '10 term at Gwinnett Technical College.

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d_alder_procedure - Diels-Alder Reaction Reference: 1....

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