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�質�學報�

è��質å��å­¸å ±å�� - 3 l...

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Unformatted text preview: 3. l 3.1. :formation of 1,2,4-trioxolane rings( ˜ Î Ê ½ ª . ) P á ‡¾ ª 6 ЉÀ D : 1H NMR spectra of untreated SO Signals increasing 1H δ (ppm) 13C δ (ppm) 5.08–5.11 (m) 104.1, 104.3 103.4, 104.4, 1.63 (bp) 30.6 1.35 (bp) 23.6, 23.7, 23.8 23.3, 23.4, Decreasing signals 1H δ (ppm) 13C δ (ppm) 5.29 (m) 127.8, 128.0, 129.6, 129.8, 130.0 –CH CHCH2CH CH– 2.72 (t) 25.6 1.96–2.03 (m) 27.1 trioxolane “*�� “* « ‘v “ ‡0� *�� � � � 3.2 Physico-chemical characterization IV: double bond PV: Ê ÍX ½ 6 ª OE: . Viscosity . 3.3. Relationships between NMR and physico-chemical measurements NMR integral value experim ental estim ated ...
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è��質å��å­¸å ±å�� - 3 l...

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