Chapter3A - 1 H NMR Spectrum 1.1 4.0 1.2 1.7 1.7 1.7 1.6...

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Unformatted text preview: 1 H NMR Spectrum 1.1 4.0 1.2 1.7 1.7 1.7 1.6 1.6 1.6 4.1 4.0 1.0 0.9 2.3 2.3 0.9 2.01 4.5 4.0 3.5 3.0 2.5 2.4 2.3 2.00 2.0 ppm 2.02 1.5 2.95 3.04 1.0 0.5 0.0 0.0 Table 3.1 Table 6.1 Figure 3.2 Figure 3.3 Figure 3.4 Figure 3.6 Figure 3.8 Figure 3.13 Figure 3.12 Figure 3.6 Figure 3.10 Figure 3.16 900 and 1000 MHz Spectrometers http://www.brukerbiospin.com http://www.oxinst.com He turret Vacuum vessel N2 turret Magnet Cross Section Radiation shield He gas N2 gas N2 vessel He vessel Liquid N2 Superconducting coil Liquid He Vibration damper Vacuum space Inner bore Magnet stand Magnet Cross Section JEOL USA, Inc Figure 3.15 Appendix G 1 H NMR Solvents Catalog No. DLM-28-25 DLM-12-25 DLM-9-25 DLM-1-25 DLM-7-50 DLM-4-25 DLM-10-25 DLM-24-25 DLM-23-25 DLM-25-10 DLM-13-25 DLM-36-10 DLM-5-25 Name 1,4-DIOXANE-D8 (P-DIOXANE) ACETIC ACID-D4 ACETONE-D6 BENZENE-D6 CHLOROFORM-D DEUTERIUM OXIDE DIMETHYL SULFOXIDE-D6 METHANOL-D4 METHYLENE CHLORIDE-D2 N,N-DIMETHYLFORMAMIDE-D7 PYRIDINE-D5 TETRAHYDROFURAN-D8 TOLUENE-D8 Isotope (D, 99%) (D, 99.5%) (D, 99.9%) (D, 99.5%) (D, 99.8%) (D, 99.9%) (D, 99.9%) (D, 99.8%) (D, 99.9%) (D, 99.5%) (D, 99.5%) (D, 99.5%) (D, 99.5%) Qty 25 G 25 G 25 G 25 G 50 G 25 G 25 G 25 G 25 G 10 G AMP 25 G 10 G AMP 25 G Price $434.00 $75.00 $45.00 $65.00 $16.00 $23.00 $43.00 $125.00 $195.00 $250.00 $122.00 $230.00 $115.00 1 H NMR Tubes Catalog No. 502-7 S-5-200-7 XR-55-7 507-HP-7 508-UP-7 S-5-600-7 Name 5 MM, 100 MHZ, 7 STANDARD SERIES 5 MM, 200 MHZ, 7 SELECT SERIES 5 MM, 300 MHZ, 7 STANDARD SERIES 5 MM, 400 MHZ, 7 STANDARD SERIES 5 MM, 500 MHZ, 7 STANDARD SERIES 5 MM, 600 MHZ, 7 SELECT SERIES Qty 50 PACK 5 PACK 25 PACK 5 PACK 5 PACK 5 PACK Price $70.00 $18.00 $79.00 $22.00 $30.50 $80.50 Appendix H Appendix H (Continued) Figure 3.16 ...
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Chapter3A - 1 H NMR Spectrum 1.1 4.0 1.2 1.7 1.7 1.7 1.6...

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