2CLabManual_2011

2CLabManual_2011 - Chemistry 2C Laboratory Manual...

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Chemistry 2C Laboratory Manual Department of Chemistry University of California - Davis Davis, CA 95616 Summer 2011
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Student Name ______________________ Locker Number____________ Laboratory Information Teaching Assistant's Name _______________________ Laboratory Section Number _______________________ Laboratory Room Number _______________________ Dispensary Room Number 1060 Sciences Lab Building Location of Safety Equipment Nearest to Your Laboratory Safety Shower _______________________ Eye Wash Fountain _______________________ Fire Extinguisher _______________________ Fire Alarm _______________________ Safety Chemicals _______________________
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i TABLE OF CONTENTS PREFACE . .................................................................................................................................. ii ACKNOWLEDGMENTS . .......................................................................................................... iii INTRODUCTION . ...................................................................................................................... iv A) Time Allocation and Grading of the Experiments . .................................................. iv B) Safety Policy . ........................................................................................................... v EXPERIMENTS: Redox Titrations . ......................................................................................................................... 1 Nomenclature of Transition Metal Complexes . .......................................................................... 9 Electrochemical Cells . ................................................................................................................. 11 EDTA Titrations . ......................................................................................................................... 23 Introduction to Inorganic Qualitative Analysis . .......................................................................... 31 Synthesis of a Transition Metal Coordination Complex . ............................................................ 39 A Spectroscopy Study . ................................................................................................................ 47 A Kinetics Study . ........................................................................................................................ 67 Determination of Vitamin C Content Via a Redox Titration. ....................................................... 75 APPENDIX: A) General Experimental Guidelines . ........................................................................... A-1 1. Pre-Laboratory Preparation . ......................................................................... A-1 2. Data Collection . ............................................................................................ A-1 3. Unknowns. .................................................................................................... A-1 4. Writing A Laboratory Report . ...................................................................... A-1
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2CLabManual_2011 - Chemistry 2C Laboratory Manual...

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