nitration_notes - and p. 637 in Bruice similar mechanism on...

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N CH 3 O H acetanilide HNO 3 H 2 SO 4 N CH 3 O H NO 2 add H 2 O which makes H 3 O + NH 3 + HSO 4 - NO 2 This material is not isolated. It is hydrolyzed. Some ortho product is present. neutralize with NH 4 OH, typical acid-base reaction not isolated NH 2 NO 2 Mechanism: see section 15.11
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Unformatted text preview: and p. 637 in Bruice similar mechanism on p. 706 of Bruice Percent yield is covered on page 12 of Bell, Clark & Taber. Recrystallization should remove any ortho product formed....
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