laboratories - - do questions 3, 4 7 Ion Exchange...

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Laboratory Experiments Do six of the following experiments: Lab Drawe r Experiment 1 Synthesis and NMR Characterization of [Cl 3 P-N(iBu)] 2 . - collect 31 P, 1 H, 13 C NMR - do questions on handout. 2 Stability Constants of Ni(glycinate) n (2-n)+ - do question 1. 3 Synthesis and IR, NMR and Melting Point Characterization of [C 5 H 5 Fe(CO) 2 ] 2 . - collect 1 H and 13 C NMR and IR - do questions 3, 5, and 7. 4 Synthesis and Characterization (IR and Melting Point) of (CH 3 ) 3 CNH 2 :BH 3 . - collect 1 H and 13 C NMR - do questions 2, 3, 8. 5 Synthesis and Thermal Analysis of the Group IIA Metal Oxalate Hydrates - run TGA of the products, determine the onset for each decomposition and compare calculated and experimental weigh loses. - do questions 4, 5 6 Synthesis of Metal Acetylacetonates (Prep. Of Tris(2,4-pentanedionato)manganese(III)
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Unformatted text preview: - do questions 3, 4 7 Ion Exchange Separation of Ionic Complexes. Ultraviolet-Visible Spectra of CrCl 2 (H 2 O) 4 + , CrCl(H 2 O) 5 2+ , Cr(H 2 O) 6 3+- do questions 4, 6 and 7. 8 Preparation of Trialkoxyboranes. - collect 1 H and 13 C NMR and IR. - do questions 1, 2. 9 Silicone Polymers: Preparation of Bouncing Putty. - do questions 3, 4, 5. 10 Determination of Magnetic Moments in Metal-Metal Bonded Complexes: Part B, Synthesis of Copper(II) Acetate Monohydrate. do questions 1, 2. 11 Geometric Isomerism (Synthesis of cis-and trans-Dichlorobis(ethylenediamine)cobalt(III) Chloride - do questions 1, 4, 12 Reaction of Cr(III) with a Multidentate Ligand: A Kinetics Experiment. - do questions 2, 3. Lab Books are due on the Following dates: Jan. 28, Feb. 25, March 25, April 29...
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This note was uploaded on 11/16/2011 for the course CHEM 3510 taught by Professor Staff during the Fall '10 term at Valdosta State University .

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