Organic Lab Reactions 47

Organic Lab Reactions 47 - 0.5 0.5 1 3 140 125 210-220...

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TABLE II— Continued orfho REARRANGEMENTS OF AIAYL AKTL ETHERS 3. MISCELLANEOUS ETHERS, DERIVATIVES OF POLTCTOLIC HYDROCARBONS Compound 2-Cinnamyloxy-3-carbomethoxy- naphthalene 1- (-y-MethylallyJoxy)-naphthalene "2-(T-Methylallyloxy)-l l 4-naphtho- quinone -4-(7-Methylallyloxy)-l,2-naphtho-^ quinone 4Hr-Ethylallyloxy)-6-hydroxy- fluoran •3,6-Di-(7-n-propylallyloxy)-fluoran 1,4-Difarnesyloxy naphthalene Conditions Time, hours Distil] Tempera- ture, °C. ation in vacuum Distillation in vacuum
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Unformatted text preview: 0.5 0.5 1 3 140 125 210-220 190-200 Solvent _ v Diethylaniline, acetic anhydride Product Ha-Phenylallyl)-2-hydroxy-3-carbomethoxynaphthalene 2-(o-Methylallyl)-l-naphthol 3-(-Methylallyl)-2-hydroxy-l,4-naphthoquinone Same compound as above 2-Pentenylfluorescein 2,7-Dihexenylfluorescein 2,3-Dif arnesyl-1,4-diacetoxynaph-thalene (?) Yield >85% >85% Reference * 115 36,124 126 126 122 122 83...
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This note was uploaded on 11/20/2011 for the course CHM 2210 taught by Professor Reynolds during the Fall '01 term at University of Florida.

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