Organic Lab Reactions 50

Organic Lab Reactions 50 - 220 Product H O CH 2 CH=CH 2...

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B. Ethers Containing Substituted AUyl Groups 1. BENZENE DERIVATIVES 7 2 8 « or"S 20 O Substituents in AUyl Group a-Ethyl /9-Methyl < 7-Phenyl 7-Methyl 7-Ethyl 7,7-Dimethyl Ring 2-Carbomethoxy- 6-methyl 2-(/3-Methylallyl)- 6-methyl 2-Carbomethoxy- 6-methyI 2-Carbomethoxy- 6-methyl 2-Carbomethoxy- 6-methyl 2-Methoxy Time, hours * 0.5 4 3 3 2.5 Conditions Tempera- ture, °C. (Alkaline Solvent (or Other Special Condition) \ rydrolysis) 210-235 Diethylaniline Diethylaniline (Refluxing diethylaniline) (Refluxing diethylaniline)
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Unformatted text preview: 220 Product H O CH 2 CH=CH 2 Substituents in Allyl Group 7-Ethjl /3-Methyl 7-Phenyl 7-Methyl 7-Ethyl 7,7-Dimethyl Ring 2-Carbomethoxy-6-methyl 2-(e-Methyla)lyl)-6-methyl 2-Carbomethoxy-6-methyl 2-Carbomethoxy-6-methyl 6-Carbomethoxy-2-methoxy 2-Methoxy Yield 70-80% 85% 59% + Refer-ence * 6,7 66 3 3 6,7 30 * Beferenoes 104-129 appeat on p. 48. t The pure product was not isolated....
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This note was uploaded on 11/20/2011 for the course CHM 2210 taught by Professor Reynolds during the Fall '01 term at University of Florida.

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