Organic Lab Reactions 52

Organic Lab Reactions 52 - 2,4,6-Triallylphenol...

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7 Allyl Group None None None None -y-Methyl C. Rearrangements -0HCH.OQ Substituents in Ring 2,6-Diallyl-4-fonnyl 2-Methoxy-4-formyl-6-allyl , 2,6-DiallyI-4-carboxy 2,6-Dimethoxy-4-carbomethoxy 2,6-Dichloro~4-carboxy Involving Displacement Conditions - Time, hours _ Temperature, >170 >180 150-300 (Heating 10 hr. with 2 N NaOH) 1.5 165-175 Product
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Unformatted text preview: 2,4,6-Triallylphenol 4,6-Diallyl-2-methoxyphenol 2,4,6-Triallylphenol 4-AUyl-2,6-dimethoxyphenol 4-Crotyl-2,6-dichlorophenol (2,6-Dichloro-4-carboxyphenoI) Yield 50% 58% >85% >85% 75% 10% Refer-ence * 44 (p. 108) 44 (p. 118) 44 (p. 91) 73 46 46 * References 104-129 appear on p. 48....
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