Organic Lab Reactions 84

Organic Lab Reactions 84 - M.p. -20, b.p. 162.5 M.p. -95.4,...

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CiF4Br 8 djF 4 Cl2 C2F 2 O2 CjF 4 O C 2 C1F S QiFe C 2 F«N 2 C 2 HFBra0 CjHFBraOz C!!HFBr 2 C2HFBr 2 C!!HFBr 2 Cl 2 QjHFBrisO C 2 HFBr 2 0 2 C 2 HFBr 4 C^FGU C»HFCa»O CjHFCl^ CWFCI4 CF-jBrCF^r CF 2 C1CF 2 C1 CF 3 CFa 2 (COF) 2 CF3COF CF 3 N=NCF 3 CHFBrCOCl CFClBrCO^ CBrF=CHBr CHF=CBr 2 CHClBrCClFBr CCl 2 BrCHFBr CHBr 2 COF CHFBrCOBr CFBr 2 CO 2 H CBr^CHB^ CBr 3 CHBrF CC12=CPF CHC1=CC1F CHC1 2 COF CFC1 2 CO 2 H CHCIFCCI3 M.p. -112°, b.p. 46.4°, d ss 2.149 M.p. -94°, b.p. 3.8°, d°1.5312, n°1.3073 B.p. about -2 ° B.p. 26° B.p. -59° M.p. -106°, b.p. -38° M.p. -106°, b.p. -79° M.p. -133° B.p. 98°, d u 1.879 M.p. -5°, b.p. 182° B.p. 88.8°, d"2.2898 B~.p. 90.3°, <Z 17 2.2908, n 17 1.4954 B.p. 163.5°, d M 2.2833, n n B.p. 163.5°, d^.lSOl B.p. 112.5°, d lo 2.3314 M.p. 26.5°, b.p. 198° B.p. 211°, <2 17 2.9094 B.p. 204°, d 16 1.9386, n 16 1.59707 M.p. -108.8°, b.p. 37.3°, ^1.3833, n 20 1.40364 B.p. 35.1°, d 16 1.4032, n 16 1.372 B.p. 70.5°, d 17 1.4802, n 17 1.3961 -
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Unformatted text preview: M.p. -20, b.p. 162.5 M.p. -95.4, b.p. 116.7&gt;d 20 1.6253, n 20 1.4525 C2F4 + Br 2 QjCle + SbF 3 Cl 2 By-product of preceding CH 3 COCHs + F 2 CFsCOjiNa at 340 C2CI6 + SbF 2 Cl 2 ; QsHsCl + F 2 Electrolysis of CF 3 CO2Na; C 2 H 4 + F 2 AgCN + F 2 CHFBrCOiiH + PQ 6 CFClBrCO 2 C 2 H6 + KOH . CBr 2 FCH 2 Br + KOH CHF 2 CHBr 2 + NaOCiiHs; CHFBrCHBr 2 + KOH CHC1=CC1F + Br 2 CCIi!=CHF + Br 2 CBrF=CHBr + (O) CBr 2 =CHF + (0) CBrF=CBrF + (0) CBr 2 CHBr 2 + SbF 3 + Br 2 CBr 2 =CHF + Br 2 CHClFCCls + Zn CHC^CCl^ + Zn CHC1 2 COC1 + SbF 3 Cl 2 CFC1 2 COC1 + H 2 O CHF=CC1 2 + Cl 2 27 27 27 63 85 27,62 57,87 119 82 113 94 114 28 82 114 82 83 94_ 94 28 28 12 23 28 * References 97-153 appear on pp 92-93....
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