Organic Lab Reactions 86

Organic Lab Reactions 86 - B.p. 60, a^l.473, n M 1.3690...

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QjHsFBr C2H 2 FBrClNO C2HisFBrCl 2 CjHsFBrOs C2H 2 FBr 2 NO C2H 2 FBr 3 CjH 2 FCl C2H2FCI2NO CjHjFCa^ CaHsFIOj C2H2FN C2H2F2 CzH^BrCl C2H 2 F2Br2 C2H 2 F 2 C1NO C 2 H 2 F 2 C) 2 CHjpOFBr CHF=CHBr CFClBrCONH 2 CHClBrCHCIF CHjjBrCGlzf CHFBrCOaH CFBr 2 CONH 2 CHBr 2 CHFBr CH 2 BrCBrtF CHs=CClF CHF=*CHC1 CFCljCONH-s CH 2 ClCa2F CHOjCHFCl CHIFCOsH CHjFCN "- CH2==CF 2 CHClBrCHF 2 CHF 2 CHBr 2 CF 2 BrCH 2 Br CF 2 C1CONH 2 COT 2 CHCl 2 , B.p. 12.5° or 6.8° or 30-35° B.p. S6° or 39.6°, <J 16 1.7097 or 1.7566, ra 16 1.4063 or 1.4204 M.p. 131.5°/ B.p. 124.7-125.1°, d S0 1.932, n 20 1.4776 B.p. 110.8°, tf 6 lM72, n 25 1.4626 M.p. 49°, b.p. 183° M.p. 136° B.p. 174°, d n 2.6709, n ls 1.5638 B.p. 1«3°, (i 17 2.6054, ft 17 1.54321 B.p. -25.5° B.p. 10-11° M.p. 126.5°, b.p. 215° M.p. -104.r,b.p.88.8°,d 2(l 1.4921, n M 1.4248 B.p. 102°, <J 17 1.54S7, n"l.5492 M.p. 74° B.p. 82°, d"1.0730 B,p. -83° B.p. 82.4°, 0*1.879, n 20 1.4173 B.p. 107.5°, (P2.3120, n^l^SSO M.p. -58°, b.p. 93°, d 17 2.24223, n 17 1.44815 M.p. 78.5°, b.p. 93718 mm.
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Unformatted text preview: B.p. 60, a^l.473, n M 1.3690 CHBrFCHjBr + CHsCOaK + K2CXJ, at 60; CFBrsCH 2 Br + Zn CHFaCHBrs + Zn From the acid CHGlBrCHOBT + SbFs + Brg CH2BrCCl8Br + HgFa CHFBTCOBT + ice CFBr2CO2C2H5 + concentrated aqueous NH CHBr 2 CHBr 2 + HgF 2 CBr 3 CH 2 Br + SbF 3 + Br 2 CHjBrCClaP + Zn CHF 2 CHCSa + Zn; CHC1FCHC1 2 + Zn Ester -f NH 4 OH CHjClCGla + BbF s + SbCfe CHCIsCHCl2 + S s F 3 + SbCl 6 CHBrFCOjC^HB + KI and saponify C H J F C O N H J + P A CHF 2 CH 2 Br + NaOC 2 H 6 ; CH 2 BrCHF 2 Br CHClBrCHClBr + SbF 3 + Br 2 CHBr 2 CHBr 2 + HgF 2-CBraCHaBf + SbFa + Brj Ester + NH 3 CHCI2CHCI2 + SbF 3 + SbCls 12,94 114, 117 82 36 Sa 82 117 38 121 5a 82 33 28 82 82 85 122,5a 36 39 94,1-21 81 82 * References 97-153 appear on pp. 92-93. SB...
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This note was uploaded on 11/20/2011 for the course CHM 2210 taught by Professor Reynolds during the Fall '01 term at University of Florida.

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