Organic Lab Reactions 262

Organic Lab Reactions 262 - Aniline Acetanilide...

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COMPOUNDS PREPARED BY THE REACTIONS 257 TABLE OP COMPOUNDS PREPARED BY THE REACTIONS— Continued Product 3,4-Dicarbometh- oxy-s'-ehloro 2-Cyano-5-methyl- 2',5'-dimethoxy 2-Cyano-5-methyl- 2',5'-diethoxy 2-Cyano-5-methyl- 2', 5'-dimethoxy- 4'-w-amyl Component A Methyl 4-amino- phthalate 2-Cyano-5-methyl- acetanilide 2-Cyano-5-methyl- acetanilide 2-Cyano-5-methyl- acetanilide Component- B Chlorobenzene p-Dimethoxy- benzene p-Diethoxy- benzene 2,5-Dimeth- oxy-n-amyl- benzene Method A-1 B-l * B-l B-l Yield 43% f 41% % 24% 27% % Refer- ence * 50 14 14 14 Terphenyls and Derivatives m-Terphenyl p-Terphenyl 2-Methyl 2-Nitro 2-, 3-, and 4- chloro 2-, 3-, and 4- bromo 4-Methyl 3-Acetamidobiphenyl Diacetyl-l,3-phenyl- ene diamine p-Aminobiphenyl
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Unformatted text preview: Aniline Acetanilide •4-Acetamidobiphenyl Diacetyl-1,4-phenyl-ene diamine. 2-Methyl-4'-acetamido-biphenyf 2-Nitro-4'-acetamido-biphenyl 4-Acetamidobiphenyl 4-Acetamidobiphenyl 4-Acetamidobiphenyl 4-Methyl-4'-acetamido-biphenyl Benzene Benzene Benzene Biphenyl Biphenyl Benzene Benzene Benzene Benzene Nitrobenzene Chlorobenzene Bromobenzene Benzene B-l B-2 B-2 A-1 A-1 B-l B-l B-l B-2 B-l B-l B-l B-l B-l B-l 24% 32% 21% 50% J 55-60%: 55-60%: 17% 25% 33% t 31% t 54% 55 8 8 3 13 58 8, 58 8 58 67 58 58 58 58 67 * References 59-76 appear on p. 261. t The product was a mixture of isomers. X Based on the nitrosoacetylamine....
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