Organic Lab Reactions 265

Organic Lab Reactions 265 - o-Nitroaniline m-Anisidine...

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260 THE PREPARATION OF UNSYMMETRICAL BIARYLS TABLE OF COMPOUNDS PSEFABED BY THE REACTIONS— Continued Product a;-(2'-Carboamyl- oxynaphthyl- 2-naphthaIene s;-(l'-Carboamyl- oxynaphthyl- 2-naphthaJene Component A /9-Acetamidonaphtha- lene 0-Acetamidonaphtha- lene Component B Amyl 2-naph- thoate Amyl 1-naph- thoate " Method B-1 B-1 Yield Refer- ence * 73 73 Arylthiophenes Phenylthiophene 8'-Cyano 4'-Nitro 4'-Chloro 4'-Bromo Aniline Acetanilide m-Cyanoaniline p-Nitroaniline p-Chloroaniline p-Bromoaniline Thiophene Thiophene Thiophene Thiophene Thiophene ThiopEene A-1 B-1 A-1 A-1 A-1 A-1 U% 15% 23% • 24% 20% 3 1 3 3 3 3 Arylpyridines Phenylpyridines 2-Methoxy 2-Nitro 3-Methoxy 3-Nitro 4-Carboxy 4-Methoxy 4-Ethoxy 4-Nitro 4-Amino 4-Chloro 4-Bromo 3-Nitro-4-meth- oxy 4-Nitro-2-meth- oxy Aniline Acetanilide o-Anisidine
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Unformatted text preview: o-Nitroaniline m-Anisidine ro-Nitroaniline p-Aminobenzoic acid p-Anisidine p-Phenetidine p-Nitroaniline Diacetyl-1,4-pheny 1-ene diamine p-Chloroaniline p-Bromoaniline 3-Nitro-4-methoxy-aniline 4-Nitro-2-methoxy-aniline Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine Pyridine A-5 B-1 A-5 A-5 A-5 A-5 A-5 A-5 A-5 A-5 B-1 A-5 A-5 A-5 A-5 40% f 60% ft 50% f 35% f 30% t 35% f 83% f 54% j 36% f 70% t 13% f 36% f 17% t 26% f 21% t 20 19 75 20 75 20 74 75 74 20 19 74 74 75 75 * References 59-76 appear on p. 261. t The produot was a mixture of isomers. X Based on the nitrosoacetylanune....
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This note was uploaded on 11/20/2011 for the course CHM 2210 taught by Professor Reynolds during the Fall '01 term at University of Florida.

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