Organic Lab Reactions 266

Organic Lab Reactions 266 - M Cook and Cook, J. Am. Chem....

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COMPOUNDS PREPARED BY THE REACTIONS 261 TABLE OF COMPOUNDS PHEPARED BY THE REACTIONS— Continued Product 5-Nitro-2-meth- oxy 3-a-Pyridylbi- phenyl 3-|8-PyridyIbi- phenyl 3-T-Pyridylbi- phenyl 3-Pyridylbi- phenyls " 4-a-Pyridylbi- phenyl 4-0-Pyridylbi- phenyl 4-7-Pyridylbi- phenyl 4-Pyridylbi- phenyls Component A 5-Nitro-2-methoxy- aniline 3-a-Pyridylacetanilide 3-/3-Pyridylacetanilide 3-y-Pyridylacetanilide 3-Aminobiphenyl 4-a-Pyridylacetanilide 4-j3-Pyridylacetanilide 4-Y-Pyridylacetanilide 4-Aminobiphenyl Component B Pyridine Benzene Benzene Benzene Pyridine Benzene Benzene Benzene Pyridine Method A-5 B-2 B-2 B-2 A-5 B-2 B-2 B-2 A-5 Yield 20%* 36% 33% 36% 39%* 40% 38% 38% 35%* Refer- ence 75 76 76 76 76 76 76 76 ' 76 * The product was a mixture of isomers. 89 Butterworth, Heilbron, Hey, and Wilkinson, / . Chem. Soc., 1938, 1386. 60 Huntress and Seikel, J. Am. Chem. Soc, 61, 820 (1939). n Suter and Smith, J. Am. Chem. Soc, 61, 166 (1939).
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Unformatted text preview: M Cook and Cook, J. Am. Chem. Soc, 55, 1216 (1933). Grieve and Hey, J. Chem. Soc, 1932, 2247. M Grieve and Hey, J. Chem. Soc, 1932, 1888. 65 Schoepfle and Truesdail, J. Am. Chem. Soc, 69, 375 (1937). M Case and Sloviter, J. Am. Chem. Soc, 59, 2381 (1937). 67 France, Heilbron, and Hey, J. Chem. Soc, 1939, 1283. 68 Case, J. Am. Chem. Soc, 60, 424 (1938). Hey, / . Chem. Soc, 1933, 2636. 70 Heilbron, Hey, and Wilkinson, J. Chem. Soc, 1938, 700. Badda];, J. Chem. Soc, 1941, 310. 78 Hey and Lawton, J. Chem. Soc, 1940, 384. . 78 Swain and Todd, / . Chem. Soc, 1941, 677. 74 Butterworth, Heilbron, and Hey, J. Chem. Soc, 1940, 365. 78 Haworth, Heilbron, and Hey, J. Chem. Soc, 1940, 358. 7 Heilbron, Hey, and Lambert, J. Chem. Soc, 1940, 1279....
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