Organic Lab Reactions 305

Organic Lab Reactions 305 - all give benzene in 60% yield....

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TABL£ II ETHANOL DEAMINATIONS CO © o 1 Amine Aniline Benzidine «-Naphthylamine j8-Naphthylamine o-Toluidine m-Toluidine ' p-Toluidine Product, Yield Phenetole (61%) + benzene (5%) Biphenyl (80%) Naphthalene (40%) + a-ethoxynaphtha- lene (23%) /S-Ethoxynaphthalene (30%) + naphtha- lene (7%) o-Methylphenetole (ca. 50%) m-Methylphenetole (ca. 40%) Toluene (ca. 45%) + p-methylphenetole {ca. 18%) Remarks Alkaline H 2 CO, NasSnC^, and HsPOj
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Unformatted text preview: all give benzene in 60% yield. H 3 PO 2 gives a 60% yield. H3PO2 gives naphthalene in 35-45% yield. H 3 PO2 gives pure toluene in 70-75% yield. Alkaline HCHO gives 80% of pure toluene. H3PO2 gives a 45% yield of pure toluene. H 8 PO 2 gives 80-85% of pure toluene. AlkaUne HCHO gives an 80% yield of pure toluene. Reference* 11, 10 14 12 12, 13 10, 13 10 10,13 o...
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This note was uploaded on 11/20/2011 for the course CHM 2210 taught by Professor Reynolds during the Fall '01 term at University of Florida.

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