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Unformatted text preview: sources (notebook page on which the compound was made or company from which it was purchased, including lot number and date), equivalents used, amounts used (mmol and weight or volume), and any relevant physical properties (density, boiling point, etc.). 4. A detailed procedure, including observations made during the reaction and a sketch of the experimental apparatus if it consists of more than simply a flask. 5. The yield of the reaction, including melting point if the product is a solid. 6. Copies of TLC plates, labeled with the eluent solvent system, developing method, identifiable spots, and R f values. 7. A list of spectra taken, where each spectrum is labeled with the notebook page on which the corresponding experimental appears. VI VII VIII...
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This note was uploaded on 01/03/2012 for the course CH 5a taught by Professor List during the Fall '10 term at Caltech.
- Fall '10