Chem 240 Lab Manual and Problem Set 2011

Chem 240 Lab Manual and Problem Set 2011 - LABORATORY...

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Unformatted text preview: LABORATORY MANUAL ORGANIC CHEMISTRY 240 FOURTH EDITION Dr. Steven Fawl LABORATORY MANUAL ORGANIC CHEMISTRY 240 FOURTH EDITION Dr. Steven Fawl Mathematics and Science Division Napa Valley College Napa, California TABLE OF CONTENTS Syllabus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Organic Chemistry 240 Lab Schedule . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 EXPERIMENT ONE - Covalent Bonding and Molecular Models . . . . . . . . . . . . . . . . . . . . . . . . 7 EXPERIMENT TWO - Isolation of Caffeine from Vivarin . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 EXPERIMENT THREE - Simple and Fractional Distillations . . . . . . . . . . . . . . . . . . . . . . . . . . 15 EXPERIMENT FOUR - Kinetics Lab: Solvolysis Effects on SN1 Reactions . . . . . . . . . . . . . . 33 EXPERIMENT FIVE- Synthesis of Cyclohexene from Cyclohexanol . . . . . . . . . . . . . . . . . . . . 37 EXPERIMENT SIX - Synthesis of Butyl Bromide from Butyl Alcohol . . . . . . . . . . . . . . . . . . . 42 EXPERIMENT SEVEN - Williamson Ether Synthesis-Butyl Methyl Ether . . . . . . . . . . . . . . . 49 N A P A V A L L E Y C O L L E G E CHEMISTRY 240 SYLLABUS COURSE : Chemistry 240 INSTRUCTOR : Dr. Steven Fawl, Room 1843, 253-3195 EMAIL [email protected] WEBSITE http://www.napavalley.edu/people/sfawl LECTURES : MW 9:30 to 10:50 Room 1638 LABS : Mon & Tues. 2:00 to 4:50 Room 1844 OFFICE HRS: M - 12:00 - 1:30, TW - 12:30 - 1:30, Th - 12:00-1:00 in MESA LABORATORY : You will be required to fill out and turn out the worksheets provided with each lab. The labs are due one week after the completion of the experiment. You must submit separate reports if working in pairs. Safety goggles will be provided in the lab but it is recommended that you buy your own pair of safety goggles which are available from the bookstore. HOMEWORK : Homework will not be specifically assigned but the problems at the end of the chapter should be done and are indicative of the problems found on the exams. Homework is not to be turned in, and will not be graded. EXAMS : Three exams and a final will be given. The following are tentative dates for your exams and the chapters each exam will cover. EXAM 1- Sept. 21 st , 2011 Alkane Nomenclature, Lewis Structures, Isomers, Newman Projections, Rotational Energy Diagrams, Hybridization, Sigma & Pi bonds, Bond shapes, Free Radical Halogenation EXAM 2- Oct. 26 th , 2011 Nucleophiles & Nucleophilic Reactions, SN1, SN2, E1, E2 Reactions, Addition Reactions, Markovnikov’s Rule, Mechanism’s, Syntheses EXAM 3- Nov. 30 th , 2011 Chemistry of Alcohols, Ethers, and Epoxides FINAL- Wednesday, Dec. 14 th , 2011 from 8:00 am to 10:00 am....
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Chem 240 Lab Manual and Problem Set 2011 - LABORATORY...

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