My H NMR for report - AV-500 new TBI(HXP probe 1D 1H starting parameters 051606 HvH Set DS=0 RN AV-500 new TBI(HXP probe 1D 1H starting parameters

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Unformatted text preview: AV-500 new TBI(HXP) probe 1D 1H starting parameters 051606 HvH. Set DS=0 1/10/07 RN AV-500 new TBI(HXP) probe 1D 1H starting parameters 051606 HvH. Set DS=0 1/10/07 RN 7.8 7.7 7.6 ppm 3671.85 3663.28 3657.21 3648.69 3634.88 1.00 1.43 7.5 7.4 7.3 7.2 7.1 16 15 14 13 12 11 10 9 8 7 0.60 2.01 2.01 1.00 1.43 1.00 2339.74 3921.54 3913.21 3767.57 3759.23 3671.85 3663.28 3657.21 3648.69 3634.88 4995.38 7.9 2.01 2.01 3767.57 3759.23 3921.54 3913.21 The chemical shifts of my proton NMR do not match those of the predicted. Furthermore, the integration values add up to only 8 hydrogens, while the expected product should have 9. This may be caused by some undesired side reaction or contamination of the product. 6 ppm 5 4 3 2 1 0 -1 -2 -3 -4 ...
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This note was uploaded on 04/07/2012 for the course CHEM 3BL taught by Professor Chunmei during the Spring '08 term at University of California, Berkeley.

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