Orgo 2 Lab 1.docx - Cat Olson CHEM 2204 TA Vasant Chary Lab...

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Cat OlsonLab Performed: 8/31/2020CHEM 2204Lab Due: 9/14/2020TA: Vasant CharyExperiment 15: The Diels-Alder Reaction: 9,10-Dihydroanthracene-9,10- α,β succinic AcidAnhydrideObjectiveIn this experiment, we learned how to use a drying tube. The overall purpose of the experiment was to investigate how Diels-Alder reactions occur with aromatic ring systems and diene substrates. Experimental ProcedureThe procedure was followed as described in Mayo’s manual pages 269-273, with the modifications listed in the “Diels Alder Modifications document” provided on Canvas. No further modifications were made to the experiment. Reaction Scheme+Anthracene Maleic anhydrideData and ResultsData and Results TableAnthraceneMaleicAnhydrideXylenes9, 10-Dihydroanthracene-9,10-α,β-succinic acid anhydrideMol. FormulaC14H10C4H2O3C18H12O3Amount (mg)864582Amount (mL)1.0mmoles.482.459Molar Mass (g)178.2498.06276.28Density.86lit. bp (°C)137-140lit. mp (ºC)21660261-262SDSFlammable,irritantHealthhazard,corrosiveHealthhazard,toxicXylenesReflux9, 10-Dihydroanthracene-9,10-α,β-succinic acid anhydride

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