Separation Process Principles- 2n - Seader & Henley - Solutions Manual

Separation Process Principles 2n Seader& Henley Solutions Manual

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Unformatted text preview: s in Example 5.4 for distillation at 400 psia of a superheated vapor feed at 105oF and containing, lbmol/h of 160 C1, 370 C2, 240 C3, 25 nC4, and 5 nC5 in a column with a partial condenser, 5 equilibrium rectification stages, equilibrium feed stage, 5 equilibrium stripping stages, and a partial reboiler, for an external reflux rate of 1,000 lbmol/h. Assumptions: No changes in absorption and stripping factors when numbers of equilibrium stages are changed. Find: Molar ratio of C3 flow rate in the distillate to that in the bottoms, with a plot, for (a) 10 rectification and 10 stripping stages, and (b) 15 rectification and 15 stripping stages. Analysis: Using the Edmister group method, the ratio of d to b for any component is given by a rearrangement of Eq. (5-66), d1 = b AF From Eqs. (5-48) and (5-50), S B φ AX + 1 / φ SX A −1 A N +1 − 1 S −1 φ S = N +1 S −1 φA = (1) AC φ SE + 1 / φ AE (2) (3) where A = L/KV and S = KV/L. In Eq. (1), φAX and φSX pertain to the stripping (exhauster)section, φAE and φSE pertain to the rectifying (enricher) section. Assume that all absorption and stripping factors are unchanged from the values given for Example 5.4. Recalculate the φ factors from Eqs. (2) and (3) for Case (a), where N = 10 for each section and Case (b), where N = 15 for each section. Analysis: (continued) Exercise 5.22 (continued) Factor φAE φAX φSE φSX N =5 0.0289 0.028 0.435 0.439 N = 10 0.00185 0.00176 0.420 0.424 N = 15 0.000123 0.000113 0.419 0.423 Using Eq. (1) with the above phi factors and the absorption and stripping factors from Example 5.4, as given below, the following d/b ratios for C3 are obtained: Factor Example 5.4 AC 10.48 AE 1.72 SE = 1/AE 0.581 AF 1.108 AX 1.73 SX = 1/AX 0.577 SB 2.78 Case d/b for C3 Example 5.4 0.0114 (a) 0.000733 (b) 0.0000487 As the number of stages increases, the separation is greatly enhanced. Exercise 5.23 Subject: Light hydrocarbon distillation by the Edmister group method. Given: Column feed at 225oF and 250 psia, corresponding to approximately 23 mol% vapor, with component flow rates below. Distillate rate is 230 kmol/h to give a separation between C3 and nC4. Column operates at 250 psia with a partial condenser and a reflux ratio of 5.0. Column contains 14 theoretical stages, with feed to stage 8, counting up from the bottom. Find: Compositions of the distillate and bottoms. Analysis: Using the DISTL (Edmister method) model of ASPEN PLUS with the ChaoSeader method for K-values, the results, with a computed 25.4 mol% vaporization, are: kmol/h: Component Feed Distillate Bottoms C2 30 29.999 0.001 C3 200 192.663 7.337 nC 4 370 7.325 362.674 nC 5 350 0.012 349.988 nC 6 50 0 50.000 Total 1,000 229.999 770.000 Exercise 5.24 Subject: Light hydrocarbon distillation by the Edmister group method. Given: Bubble-point column feed at 120 psia, with component flow rates below. Distillate rate is 45 kmol/h to give a separation between nC4 and iC5. Column operates at 120 psia with a partial condenser and a boilup of 200 kmol/h Column contains 20 theoretical stages, with feed to stage 10, counting up from the bottom. Find: Compositions of the distillate and bottoms. Analysis: Using the DISTL (Edmister method) model of ASPEN PLUS with the ChaoSeader method for K-values, and a reflux rate of 200 - 45 = 1...
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This document was uploaded on 02/24/2014 for the course CBE 2124 at NYU Poly.

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