Remove the solvent using a rotary evaporator and

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Unformatted text preview: iodically. Drain the aqueous layer into a clean 100 mL beaker. Extract the organic layer with another 25 mL of the sodium hydroxide solution and drain the aqueous layer into the same beaker. Collect the organic layer in a separate 125 mL Erlenmeyer flask. Cool the aqueous layer in an ice- water bath and acidify with 6M aqueous hydrochloric acid. Return the acidified solution to the separatory funnel and extract with 15 mL of hexanes. Shake the funnel for about a minute...
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